C₄₁H₄₇N₃O₇

Base Information

Chemical Name:C₄₁H₄₇N₃O₇
CAS No.:1421917-00-1
Molecular Formula:C₄₁H₄₇N₃O₇
Molecular Weight:693.84
Hs Code.:

C<sub>41</sub>H<sub>47</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₄₁H₄₇N₃O₇

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Chemical Property of C₄₁H₄₇N₃O₇

Chemical Property:

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Technology Process of C₄₁H₄₇N₃O₇

There total 17 articles about C₄₁H₄₇N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421916-99-5
C₄₁H₄₇BrO₇

: 1421917-00-1
C₄₁H₄₇N₃O₇

Guidance literature:: With tetramethylguanidinum azide; In nitromethane; at 0 - 25 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.steroids.2012.10.021

Reference yield:

: 227178-66-7
3β-acetoxy-12β-hydroxy-5α-spirostan-14-ene

: 1421917-00-1
C₄₁H₄₇N₃O₇

Guidance literature:: Multi-step reaction with 13 steps

1: pyridine / 6 h / Inert atmosphere

2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 19 h / 0 - 25 °C / Inert atmosphere

3: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

4: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere

5: hydroquinidein 1,4-phthalazinediyl diether; potassium carbonate; potassium hexacyanoferrate(III); potassium osmate(VI) / water; tert-butyl alcohol / 18 h / 0 °C / Inert atmosphere

6: 1H-imidazole; dmap / dichloromethane / 1 h / 25 °C / Inert atmosphere

7: triethylamine; magnesium dibromide etherate / dichloromethane / 2 h / 25 °C / Inert atmosphere

8: boron trifluoride diethyl etherate / dichloromethane / 1 h / Inert atmosphere

9: iodine; [bis(acetoxy)iodo]benzene / dichloromethane; cyclohexane / 6 h / 0 °C / Inert atmosphere

10: potassium carbonate / methanol; water / 12 h / 25 °C / Inert atmosphere

11: Jones reagent / acetone / 0.33 h / 0 °C / Inert atmosphere

12: phenyltrimethylammonium tribromide / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

13: tetramethylguanidinum azide / nitromethane / 6 h / 0 - 25 °C / Inert atmosphere

With pyridine; 1H-imidazole; triethylsilane; dmap; potassium osmate(VI); Jones reagent; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; iodine; phenyltrimethylammonium tribromide; potassium carbonate; magnesium dibromide etherate; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; triphenylphosphine; tetramethylguanidinum azide; potassium hexacyanoferrate(III); In tetrahydrofuran; methanol; nitromethane; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1016/j.steroids.2012.10.021

Reference yield:

: C₄₂H₆₄O₇Si

: 1421917-00-1
C₄₁H₄₇N₃O₇

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine; magnesium dibromide etherate / dichloromethane / 2 h / 25 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 1 h / Inert atmosphere

3: iodine; [bis(acetoxy)iodo]benzene / dichloromethane; cyclohexane / 6 h / 0 °C / Inert atmosphere

4: potassium carbonate / methanol; water / 12 h / 25 °C / Inert atmosphere

5: Jones reagent / acetone / 0.33 h / 0 °C / Inert atmosphere

6: phenyltrimethylammonium tribromide / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

7: tetramethylguanidinum azide / nitromethane / 6 h / 0 - 25 °C / Inert atmosphere

With Jones reagent; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; iodine; phenyltrimethylammonium tribromide; potassium carbonate; magnesium dibromide etherate; triethylamine; tetramethylguanidinum azide; In tetrahydrofuran; methanol; nitromethane; dichloromethane; cyclohexane; water; acetone;
DOI:10.1016/j.steroids.2012.10.021