Technology Process of C20H23NO3
There total 10 articles about C20H23NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol; ethyl acetate;
at 20 ℃;
for 4h;
DOI:10.1021/jo052516c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / Me2AlCl / hexane; CH2Cl2 / 0.5 h / -75 - -67 °C
2: 100 percent / H2 / Pd/C / ethyl acetate; methanol / 4 h / 20 °C
With
hydrogen; dimethylaluminum chloride;
palladium on activated charcoal;
In
methanol; hexane; dichloromethane; ethyl acetate;
2: Diels-Alder reaction;
DOI:10.1021/jo052516c
- Guidance literature:
-
Multi-step reaction with 4 steps
1: oxalyl chloride
2: 80 percent / Me2AlCl / hexane; CH2Cl2 / 0.5 h / -75 - -67 °C
3: 100 percent / H2 / Pd/C / ethyl acetate; methanol / 4 h / 20 °C
With
oxalyl dichloride; hydrogen; dimethylaluminum chloride;
palladium on activated charcoal;
In
methanol; hexane; dichloromethane; ethyl acetate;
3: Diels-Alder reaction;
DOI:10.1021/jo052516c