C₅₄H₉₀N₂O₈

Base Information

• Chemical Name: C₅₄H₉₀N₂O₈
• CAS No.: 1353391-10-2
• Molecular Formula: C₅₄H₉₀N₂O₈
• Molecular Weight: 895.317
• Mol file: 1353391-10-2.mol

Synonyms:C₅₄H₉₀N₂O₈

Chemical Property of C₅₄H₉₀N₂O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₄H₉₀N₂O₈

There total 8 articles about C₅₄H₉₀N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

3,4,5-(tri-dodecyloxy)benzoylaminoethyl amide hydrochloride (1353391-09-9) + 2-(4-formyl-3-hydroxyphenoxy)acetic acid → C54H90N2O8 (1353391-10-2)

Guidance literature:

With pyridine; dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 24h;

DOI:10.1039/c1cc16232b

Reference yield:

Ethyl gallate (831-61-8) → C54H90N2O8 (1353391-10-2)

Guidance literature:

Multi-step reaction with 5 steps

1: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 72 h / Reflux

2: water; sodium hydroxide / ethanol / 3 h / 80 °C

3: thionyl chloride / dichloromethane / 3 h / 20 °C

4: tetrahydrofuran / 0 - 20 °C

5: pyridine; dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 0 - 20 °C

With pyridine; dmap; thionyl chloride; tetrabutylammomium bromide; water; potassium carbonate; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;

DOI:10.1039/c1cc16232b

Reference yield:

1-dodecylbromide (143-15-7) → C54H90N2O8 (1353391-10-2)

Guidance literature:

Multi-step reaction with 5 steps

1: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 72 h / Reflux

2: water; sodium hydroxide / ethanol / 3 h / 80 °C

3: thionyl chloride / dichloromethane / 3 h / 20 °C

4: tetrahydrofuran / 0 - 20 °C

5: pyridine; dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 0 - 20 °C

With pyridine; dmap; thionyl chloride; tetrabutylammomium bromide; water; potassium carbonate; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;

DOI:10.1039/c1cc16232b

upstream raw materials:

3,4,5-(tri-dodecyloxy)benzoylaminoethyl amide hydrochloride

Ethyl gallate

1-dodecylbromide

ethyl 3,4,5-tri(dodecyloxy)benzoate

Downstream raw materials:

C₁₁₄H₁₈₄N₆O₁₄