triisopropyl((4-((3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)ethynyl)phenyl)ethynyl)silane

Base Information

Chemical Name:triisopropyl((4-((3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)ethynyl)phenyl)ethynyl)silane
CAS No.:1609200-04-5
Molecular Formula:C₄₆H₇₂O₁₂Si
Molecular Weight:845.156
Hs Code.:

Synonyms:triisopropyl((4-((3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)ethynyl)phenyl)ethynyl)silane

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Chemical Property of triisopropyl((4-((3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)ethynyl)phenyl)ethynyl)silane

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Technology Process of triisopropyl((4-((3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)ethynyl)phenyl)ethynyl)silane

There total 7 articles about triisopropyl((4-((3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)ethynyl)phenyl)ethynyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1041859-46-4
5-bromo-1,2,3-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzene

: 175345-90-1
1-((triisopropylsilyl)ethynyl)-4-ethynylbenzene

: 1609200-04-5
triisopropyl((4-((3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)ethynyl)phenyl)ethynyl)silane

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; at 70 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201307806

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 1609200-04-5
triisopropyl((4-((3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)ethynyl)phenyl)ethynyl)silane

Guidance literature:: Multi-step reaction with 4 steps

1: trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide; triethylamine / 20 °C / Inert atmosphere

2: trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide; triethylamine / 100 °C / Inert atmosphere

3: potassium carbonate / tetrahydrofuran; methanol / 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; triethylamine / 3 h / 70 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1002/anie.201307806

Reference yield:

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 1609200-04-5
triisopropyl((4-((3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)ethynyl)phenyl)ethynyl)silane

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 °C

2: potassium carbonate / 90 - 100 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; triethylamine / 3 h / 70 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; triethylamine; In dichloromethane;
DOI:10.1002/anie.201307806