Technology Process of C23H24N4O6S
There total 6 articles about C23H24N4O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
for 0.75h;
DOI:10.1021/ja310659j
- Guidance literature:
-
Multi-step reaction with 8 steps
1: potassium hydroxide; Tris(3,6-dioxaheptyl)amine / toluene / 20 °C
2: dmap / tetrahydrofuran / 20 °C / Sealed tube
3: hydrogenchloride / tetrahydrofuran; water / 20 °C
4: pyridine / 20 °C
5: tetra-(n-butyl)ammonium iodide; sodium hydroxide / toluene; water
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C
7: N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / -50 - 20 °C
8: trifluoroacetic acid / dichloromethane / 0.75 h
With
pyridine; hydrogenchloride; dmap; Tris(3,6-dioxaheptyl)amine; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1021/ja310659j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydroxide / toluene; water
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / -50 - 20 °C
4: trifluoroacetic acid / dichloromethane / 0.75 h
With
tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1021/ja310659j
