N,N'-Bis-[1-(4-tert-butyl-2,6-dimethyl-phenyl)-meth-(E)-ylidene]-hydrazine

Base Information

Chemical Name:N,N'-Bis-[1-(4-tert-butyl-2,6-dimethyl-phenyl)-meth-(E)-ylidene]-hydrazine
CAS No.:85152-33-6
Molecular Formula:C₂₆H₃₆N₂
Molecular Weight:376.585
Hs Code.:

Synonyms:N,N'-Bis-[1-(4-tert-butyl-2,6-dimethyl-phenyl)-meth-(E)-ylidene]-hydrazine

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Chemical Property of N,N'-Bis-[1-(4-tert-butyl-2,6-dimethyl-phenyl)-meth-(E)-ylidene]-hydrazine

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Technology Process of N,N'-Bis-[1-(4-tert-butyl-2,6-dimethyl-phenyl)-meth-(E)-ylidene]-hydrazine

There total 3 articles about N,N'-Bis-[1-(4-tert-butyl-2,6-dimethyl-phenyl)-meth-(E)-ylidene]-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 85151-95-7
2,6-Dimethyl-4-tert-butylbenzaldehyde

: 85152-33-6
N,N'-Bis-[1-(4-tert-butyl-2,6-dimethyl-phenyl)-meth-(E)-ylidene]-hydrazine

Guidance literature:: With hydrazine hydrate; In ethanol; for 12h; Heating;
DOI:10.1021/jo00157a015

Reference yield:

: 85151-94-6
C₂₁H₂₈N₂O

: 85152-33-6
N,N'-Bis-[1-(4-tert-butyl-2,6-dimethyl-phenyl)-meth-(E)-ylidene]-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 5N aq. HCl / ethanol / 0.5 h / Ambient temperature

2: 69 percent / NH₂NH₂*H₂O / ethanol / 12 h / Heating

With hydrogenchloride; hydrazine hydrate; In ethanol;
DOI:10.1021/jo00157a015

Reference yield:

: 78919-93-4
1-(4-tert-Butyl-2,6-dimethyl-benzyl)-pyridinium; chloride

: 85152-33-6
N,N'-Bis-[1-(4-tert-butyl-2,6-dimethyl-phenyl)-meth-(E)-ylidene]-hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1N aq. NaOH / ethanol / 1.5 h / Ambient temperature

2: 5N aq. HCl / ethanol / 0.5 h / Ambient temperature

3: 69 percent / NH₂NH₂*H₂O / ethanol / 12 h / Heating

With hydrogenchloride; sodium hydroxide; hydrazine hydrate; In ethanol;
DOI:10.1021/jo00157a015