2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-amino-1,2-dideoxy-D-glucitol

Base Information

• Chemical Name: 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-amino-1,2-dideoxy-D-glucitol
• CAS No.: 119009-35-7
• Molecular Formula: C₁₆H₃₁N₃O₁₀
• Molecular Weight: 425.436

Synonyms:2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-amino-1,2-dideoxy-D-glucitol

Chemical Property of 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-amino-1,2-dideoxy-D-glucitol

Chemical Property:

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Technology Process of 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-amino-1,2-dideoxy-D-glucitol

There total 3 articles about 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-amino-1,2-dideoxy-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-N-(4-L-aspartoyl)-2-deoxy-β-D-glucopyranosylamine (29625-73-8) → L-homoserine (672-15-1,119736-88-8) + N,N'-diacetylchitobiosamine (102039-77-0) + 1-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-amino-1,2-dideoxy-D-glucitol (118943-00-3) + 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-amino-1,2-dideoxy-D-glucitol (119009-35-7) + β-D-GlcpNAc(1->4)-D-GlcNAc-ol (29886-32-6)

Guidance literature:

With lithium hydroxide; lithium borohydride; trilithium citrate; In water; tert-butyl alcohol; at 45 ℃; for 5h; Product distribution;

DOI:10.1016/0008-6215(88)80108-3

Reference yield: 72.0%

2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-N-(4-L-aspartoyl)-2-deoxy-β-D-glucopyranosylamine (29625-73-8) → L-homoserine (672-15-1,119736-88-8) + N,N'-diacetylchitobiosamine (102039-77-0) + 1-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-amino-1,2-dideoxy-D-glucitol (118943-00-3) + 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-amino-1,2-dideoxy-D-glucitol (119009-35-7)

Guidance literature:

With lithium hydroxide; lithium borohydride; trilithium citrate; In water; tert-butyl alcohol; at 45 ℃; for 5h; Yield given;

DOI:10.1016/0008-6215(88)80108-3

Reference yield: 72.0%

2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-N-(4-L-aspartoyl)-2-deoxy-β-D-glucopyranosylamine (29625-73-8) → L-homoserine (672-15-1,119736-88-8) + N,N'-diacetylchitobiosamine (102039-77-0) + 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-amino-1,2-dideoxy-D-glucitol (119009-35-7) + β-D-GlcpNAc(1->4)-D-GlcNAc-ol (29886-32-6)

Guidance literature:

With lithium hydroxide; lithium borohydride; trilithium citrate; In water; tert-butyl alcohol; at 45 ℃; for 5h;

DOI:10.1016/0008-6215(88)80108-3

upstream raw materials:

2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-1-N-(4-L-aspartoyl)-2-deoxy-β-D-glucopyranosylamine

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