DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol

Base Information

Chemical Name:DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol
CAS No.:104600-57-9
Molecular Formula:C₁₅H₁₇NO₅
Molecular Weight:291.304
Hs Code.:

Synonyms:DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol

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Chemical Property of DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol

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Technology Process of DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol

There total 1 articles about DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 104600-54-6
DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol 5-Acetate

: 104600-57-9
DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 13h;
DOI:10.1002/jlac.198619861201

Reference yield:

: 104600-57-9
DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol

: 104712-71-2
(1S^*)-(1α,2α,3α,4β,5β,6β)-2-O-Benzyl-5-O,6-N-carbonyl-1-O-methyl-6-(methylamino)-4-<(R)-(1-phenylethyl)amino>-1,2,3,5-cyclohexanetetrol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) glyme, 15 min; 2.) 20 deg C, 1 h

2: propan-1-ol / 72 h / Heating

With sodium hydride; In propan-1-ol;
DOI:10.1002/jlac.198619861201

Reference yield:

: 104600-57-9
DL-(1α,2β,3β,4β,5β,6α)-2,3-Anhydro-4-O-benzyl-1-O,6-N-carbonyl-6-(methylamino)-1,2,3,4,5-cyclohexanepentol

: 104619-29-6
(+)-(1R)-(1α,2α,3β,4α,5β,6β)-2-O-Benzyl-5-O,6-N-carbonyl-1-O-methyl-6-(methylamino)-3-<(R)-(1-phenylethyl)amino>-1,2,4,5-cyclohexanetetrol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) glyme, 15 min; 2.) 20 deg C, 1 h

2: 35 percent / propan-1-ol / 72 h / Heating

With sodium hydride; In propan-1-ol;
DOI:10.1002/jlac.198619861201