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Technology Process of FeC20H8N4(C6H3(COOC2H5)2)4

FeC20H8N4(C6H3(COOC2H5)2)4

Base Information
  • Chemical Name:FeC20H8N4(C6H3(COOC2H5)2)4
  • CAS No.:602329-74-8
  • Molecular Formula:C68H60FeN4O16
  • Molecular Weight:1245.09
  • Hs Code.:
FeC<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>3</sub>(COOC<sub>2</sub>H<sub>5</sub>)2)4

Synonyms:FeC20H8N4(C6H3(COOC2H5)2)4

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Chemical Property of FeC20H8N4(C6H3(COOC2H5)2)4
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Technology Process of FeC20H8N4(C6H3(COOC2H5)2)4

There total 1 articles about FeC20H8N4(C6H3(COOC2H5)2)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

iron(II) chloride hydrate

iron(II) chloride hydrate

C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>H<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>(COOC<sub>2</sub>H<sub>5</sub>)2)4

C20H8N4H2(C6H3(COOC2H5)2)4

FeC<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>3</sub>(COOC<sub>2</sub>H<sub>5</sub>)2)4
602329-74-8

FeC20H8N4(C6H3(COOC2H5)2)4

Guidance literature:
In dichloromethane; N,N-dimethyl-formamide; soln. of ligand in FeCl2*nH2O-satd. DMF was added to CH2Cl2, stirred for12 h at 50°C in the dark under N2; TLC (SiO2/CH2Cl2/ethyl acetate), solvent was removed under reduced pressure, dissolved in CHCl3, washed with water, satd. aq. NaCl, dried over Na2SO4, solvent was evapd.;
DOI:10.1021/ja035055q

Reference yield: 94.0%

FeC<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>3</sub>(COOC<sub>2</sub>H<sub>5</sub>)2)4
602329-74-8

FeC20H8N4(C6H3(COOC2H5)2)4

FeC<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>3</sub>(COOH)2)4

FeC20H8N4(C6H3(COOH)2)4

Guidance literature:
With KOH; In methanol; water; MeOH/H2O soln. of Fe-complex and KOH was refluxed for 12 h; MeOH was evapd., aq. residue was acidified to pH 1 with aq. HCl, cooled by ice, filtered;
DOI:10.1021/ja035055q
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