2-tert-butyldimethylsilyl-5-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)-N,N-dimethylimidazole-1-sulfonamide

Base Information

Chemical Name:2-tert-butyldimethylsilyl-5-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)-N,N-dimethylimidazole-1-sulfonamide
CAS No.:391249-75-5
Molecular Formula:C₃₇H₄₉N₃O₆SSi
Molecular Weight:691.964
Hs Code.:

Synonyms:2-tert-butyldimethylsilyl-5-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)-N,N-dimethylimidazole-1-sulfonamide

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Chemical Property of 2-tert-butyldimethylsilyl-5-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)-N,N-dimethylimidazole-1-sulfonamide

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Technology Process of 2-tert-butyldimethylsilyl-5-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)-N,N-dimethylimidazole-1-sulfonamide

There total 1 articles about 2-tert-butyldimethylsilyl-5-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)-N,N-dimethylimidazole-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2-(tert-Butyl-dimethyl-silanyl)-5-((1R,2S,3S,4R)-2,3,5-tris-benzyloxy-1,4-dihydroxy-pentyl)-imidazole-1-sulfonic acid dimethylamide

: 391249-75-5
2-tert-butyldimethylsilyl-5-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)-N,N-dimethylimidazole-1-sulfonamide

Guidance literature:: With tributylphosphine; diamide; In benzene; at 20 ℃; for 48h;

Reference yield: 87.0%

: 391249-75-5
2-tert-butyldimethylsilyl-5-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)-N,N-dimethylimidazole-1-sulfonamide

: 391249-76-6
4(5)-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)imidazole

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; for 1.5h; Heating;

Reference yield:

: 391249-75-5
2-tert-butyldimethylsilyl-5-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)-N,N-dimethylimidazole-1-sulfonamide

: ethyl 4-(2,3,5-tri-O-benzyl-α-D-xylofuranosyl)imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / HCl / tetrahydrofuran; H₂O / 1.5 h / Heating

2: 73 percent / pyridine; 4-DMAP / 0.33 h / Heating

With pyridine; hydrogenchloride; dmap; In tetrahydrofuran; water;