4-{[butyl(1-butyl-2-phenyl(4,5,6-trihydrocyclopenta[3,2-d]imidazol-6-yl))amino]methyl}-3-chlorophenol

Base Information

Chemical Name:4-{[butyl(1-butyl-2-phenyl(4,5,6-trihydrocyclopenta[3,2-d]imidazol-6-yl))amino]methyl}-3-chlorophenol
CAS No.:439557-47-8
Molecular Formula:C₂₇H₃₄ClN₃O
Molecular Weight:452.039
Hs Code.:

Synonyms:4-{[butyl(1-butyl-2-phenyl(4,5,6-trihydrocyclopenta[3,2-d]imidazol-6-yl))amino]methyl}-3-chlorophenol

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Chemical Property of 4-{[butyl(1-butyl-2-phenyl(4,5,6-trihydrocyclopenta[3,2-d]imidazol-6-yl))amino]methyl}-3-chlorophenol

Chemical Property:

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Technology Process of 4-{[butyl(1-butyl-2-phenyl(4,5,6-trihydrocyclopenta[3,2-d]imidazol-6-yl))amino]methyl}-3-chlorophenol

There total 6 articles about 4-{[butyl(1-butyl-2-phenyl(4,5,6-trihydrocyclopenta[3,2-d]imidazol-6-yl))amino]methyl}-3-chlorophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56962-11-9
2-chloro-4-hydroxybenzaldehyde

: 439571-74-1
butyl(1-butyl-2-phenyl-4,5,6-trihydrocyclopentyl[3,2-d]imidazol-6-yl)amine

: 439557-47-8
4-{[butyl(1-butyl-2-phenyl(4,5,6-trihydrocyclopenta[3,2-d]imidazol-6-yl))amino]methyl}-3-chlorophenol

Guidance literature:: 2-chloro-4-hydroxybenzaldehyde; butyl(1-butyl-2-phenyl-4,5,6-trihydrocyclopentyl[3,2-d]imidazol-6-yl)amine; With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane;

With water; ammonium chloride; In 1,2-dichloro-ethane;

Reference yield:

: 3859-41-4
1,3-cyclopentadione

: 439557-47-8
4-{[butyl(1-butyl-2-phenyl(4,5,6-trihydrocyclopenta[3,2-d]imidazol-6-yl))amino]methyl}-3-chlorophenol

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-Bromosuccinimide / chloroform / 2 h / Heating / reflux

1.2: Heating / reflux

2.1: potassium carbonate / chloroform; water / Heating / reflux

3.1: sodium tetrahydroborate / methanol

4.1: thionyl chloride / chloroform / 20 °C

5.1: 2 h

6.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane

With sodium tetrahydroborate; N-Bromosuccinimide; thionyl chloride; sodium tris(acetoxy)borohydride; potassium carbonate; In methanol; chloroform; water; 1,2-dichloro-ethane;

Reference yield:

: 439571-72-9
1-butyl-2-phenyl-4,5-dihydrocyclopenty[1,2-d]imidazol-6-one

: 439557-47-8
4-{[butyl(1-butyl-2-phenyl(4,5,6-trihydrocyclopenta[3,2-d]imidazol-6-yl))amino]methyl}-3-chlorophenol

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / methanol

2: thionyl chloride / chloroform / 20 °C

3: 2 h

4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane

With sodium tetrahydroborate; thionyl chloride; sodium tris(acetoxy)borohydride; In methanol; chloroform; 1,2-dichloro-ethane;