3-(3-Benzyloxycarbonylmethyl-2,4,5-trioxo-imidazolidin-1-ylmethyl)-benzoic acid methyl ester

Base Information

Chemical Name:3-(3-Benzyloxycarbonylmethyl-2,4,5-trioxo-imidazolidin-1-ylmethyl)-benzoic acid methyl ester
CAS No.:179412-45-4
Molecular Formula:C₂₁H₁₈N₂O₇
Molecular Weight:410.383
Hs Code.:

Synonyms:3-(3-Benzyloxycarbonylmethyl-2,4,5-trioxo-imidazolidin-1-ylmethyl)-benzoic acid methyl ester

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Chemical Property of 3-(3-Benzyloxycarbonylmethyl-2,4,5-trioxo-imidazolidin-1-ylmethyl)-benzoic acid methyl ester

Chemical Property:

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Technology Process of 3-(3-Benzyloxycarbonylmethyl-2,4,5-trioxo-imidazolidin-1-ylmethyl)-benzoic acid methyl ester

There total 3 articles about 3-(3-Benzyloxycarbonylmethyl-2,4,5-trioxo-imidazolidin-1-ylmethyl)-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 188624-38-6
benzyl ureidoacetate

: 179412-45-4
3-(3-Benzyloxycarbonylmethyl-2,4,5-trioxo-imidazolidin-1-ylmethyl)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / tetrahydrofuran / 4 h / 0 °C

2: 1.) NaH / 1.) DMF, 0 deg C, 1 h, 2.) DMF, 0 deg C, 2 h

With sodium hydride; In tetrahydrofuran;
DOI:10.1248/cpb.45.297

Reference yield:

: 1738-76-7
glycine benzyl ester p-toluenesulfonic acid salt

: 179412-45-4
3-(3-Benzyloxycarbonylmethyl-2,4,5-trioxo-imidazolidin-1-ylmethyl)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / AcOH, conc. HCl / H₂O / 5 h / Heating

2: 79 percent / tetrahydrofuran / 4 h / 0 °C

3: 1.) NaH / 1.) DMF, 0 deg C, 1 h, 2.) DMF, 0 deg C, 2 h

With hydrogenchloride; sodium hydride; acetic acid; In tetrahydrofuran; water;
DOI:10.1248/cpb.45.297

Reference yield:

: 1129-28-8
3-methoxycarbonylbenzyl bromide

: 188624-37-5
(2,4,5-Trioxo-imidazolidin-1-yl)-acetic acid benzyl ester

: 179412-45-4
3-(3-Benzyloxycarbonylmethyl-2,4,5-trioxo-imidazolidin-1-ylmethyl)-benzoic acid methyl ester

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 0 deg C, 1 h, 2.) DMF, 0 deg C, 2 h;
DOI:10.1248/cpb.45.297