{((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O)⁽¹⁺⁾*CF₃SO₃^(1-)=({((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O))(CF₃SO₃)

Base Information

• Chemical Name: {((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O)⁽¹⁺⁾*CF₃SO₃^(1-)=({((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O))(CF₃SO₃)
• CAS No.: 119326-09-9
• Molecular Formula: CF₃O₃S*C₄₂H₃₆NOPd
• Molecular Weight: 826.244

Synonyms:{((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O)⁽¹⁺⁾*CF₃SO₃^(1-)=({((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O))(CF₃SO₃)

Chemical Property of {((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O)⁽¹⁺⁾*CF₃SO₃^(1-)=({((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O))(CF₃SO₃)

Chemical Property:

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Technology Process of {((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O)⁽¹⁺⁾*CF₃SO₃^(1-)=({((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O))(CF₃SO₃)

There total 3 articles about {((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O)⁽¹⁺⁾*CF₃SO₃^(1-)=({((C₆H₅)4C₄)C₆H₄(C₆H₄(N(CH₃)2))}Pd(H₂O))(CF₃SO₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(N,N-dimethylamino)-1,1'-biphenyl (6590-81-4) → {((C6H5)4C4)C6H4(C6H4(N(CH3)2))}Pd(H2O)(1+)*CF3SO3(1-)=({((C6H5)4C4)C6H4(C6H4(N(CH3)2))}Pd(H2O))(CF3SO3) (119326-09-9)

Guidance literature:

Multi-step reaction with 3 steps

1: not given

2: tetrahydrofuran

3: dichloromethane

In tetrahydrofuran; dichloromethane;

Reference yield:

bis(N,N-dimethyl-2-aminobiphenyl)dipalladium-μ-dichloride (119326-02-2) → {((C6H5)4C4)C6H4(C6H4(N(CH3)2))}Pd(H2O)(1+)*CF3SO3(1-)=({((C6H5)4C4)C6H4(C6H4(N(CH3)2))}Pd(H2O))(CF3SO3) (119326-09-9)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: dichloromethane

In tetrahydrofuran; dichloromethane;

Reference yield:

{(C6H4C6H4(N(CH3)2))Pd(CH2CH2CH2CH2O)2}(1+)*CF3SO3(1-)={(C6H4C6H4(N(CH3)2))Pd(CH2CH2CH2CH2O)2}(CF3SO3) (119326-05-5) + diphenyl acetylene (501-65-5) → {((C6H5)4C4)C6H4(C6H4(N(CH3)2))}Pd(H2O)(1+)*CF3SO3(1-)=({((C6H5)4C4)C6H4(C6H4(N(CH3)2))}Pd(H2O))(CF3SO3) (119326-09-9)

Guidance literature:

In dichloromethane; treating Pd complex with excess (> 4-fold) of diphenylacetylene (5 min stirring, room temp.), addn. of pentane, pptn.;

upstream raw materials:

{(C₆H₄C₆H₄(N(CH₃)2))Pd(CH₂CH₂CH₂CH₂O)2}⁽¹⁺⁾*CF₃SO₃^(1-)={(C₆H₄C₆H₄(N(CH₃)2))Pd(CH₂CH₂CH₂CH₂O)2}(CF₃SO₃)

diphenyl acetylene

2-(N,N-dimethylamino)-1,1'-biphenyl

bis(N,N-dimethyl-2-aminobiphenyl)dipalladium-μ-dichloride

Downstream raw materials:

(C₆H₅)4C₁₀H₄(C₆H₃(NH(CH₃)2))⁽¹⁺⁾

palladium

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