L-Alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Mono(triethylammonium) Salt

Base Information

• Chemical Name: L-Alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Mono(triethylammonium) Salt
• CAS No.: 118597-45-8
• Molecular Formula: C₆H₁₅N*C₁₁H₁₅N₃O₆S
• Molecular Weight: 418.514

Synonyms:L-Alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Mono(triethylammonium) Salt

Chemical Property of L-Alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Mono(triethylammonium) Salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of L-Alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Mono(triethylammonium) Salt

There total 4 articles about L-Alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Mono(triethylammonium) Salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-Carbobenzoxy-L-alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Benzyl Ester Triethylammonium Salt (118597-40-3) → L-Alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Mono(triethylammonium) Salt (118597-45-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 1.5h; under 2585.7 Torr;

DOI:10.1021/jm00123a034

Reference yield:

N-carboxybenzoxy-L-alanyl-D,L-2-acetoxyglycine benzyl ester (89625-84-3) → L-Alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Mono(triethylammonium) Salt (118597-45-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) Et₃N, 2) Et₃N / 1) H₂O, 2) DMF, overnight

2: 97 percent / H₂ / 10percent Pd-C / methanol / 1.5 h / 2585.7 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In methanol;

DOI:10.1021/jm00123a034

Reference yield:

triethylamine (121-44-8) → L-Alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Mono(triethylammonium) Salt (118597-45-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) Et₃N, 2) Et₃N / 1) H₂O, 2) DMF, overnight

2: 97 percent / H₂ / 10percent Pd-C / methanol / 1.5 h / 2585.7 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In methanol;

DOI:10.1021/jm00123a034

upstream raw materials:

N-Carbobenzoxy-L-alanyl-D,L-2-<(4-sulfophenyl)amino>glycine Benzyl Ester Triethylammonium Salt

N-carboxybenzoxy-L-alanyl-D,L-2-acetoxyglycine benzyl ester

triethylamine

4-aminobenzene sulfonic acid

Downstream raw materials:

N-Carbobenzoxy-L-alanyl-L-alanyl-D,L-2-<(4-sulfophenyl)amino>glycine dipotassium salt

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