matairesinyl 4,4'-bistriflate

Base Information

Chemical Name:matairesinyl 4,4'-bistriflate
CAS No.:501645-95-0
Molecular Formula:C₂₂H₂₀F₆O₁₀S₂
Molecular Weight:622.517
Hs Code.:

Synonyms:matairesinyl 4,4'-bistriflate

Suppliers and Price of matairesinyl 4,4'-bistriflate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of matairesinyl 4,4'-bistriflate

Chemical Property:

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Technology Process of matairesinyl 4,4'-bistriflate

There total 2 articles about matairesinyl 4,4'-bistriflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 580-72-3,7471-01-4,42298-55-5,120409-94-1,148409-36-3
matairesinol

: 501645-95-0
matairesinyl 4,4'-bistriflate

Guidance literature:: With lutidine; In dichloromethane; at 0 ℃; for 48h;
DOI:10.1021/ol0273598

Reference yield:

: 347359-71-1
(7RS,8R,8'R)-4,4',7-trihydroxy-3,3'-dimethoxylignano-9,9'-lactone

: 501645-95-0
matairesinyl 4,4'-bistriflate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent Turnov_. / H₂ / Pd/C / 1,2-dichloro-ethane / 4 h / 50 °C / 6000.6 Torr

2: 88 percent / lutidine / CH₂Cl₂ / 48 h / 0 °C

With lutidine; hydrogen; palladium on activated charcoal; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol0273598

Reference yield:

: 501645-95-0
matairesinyl 4,4'-bistriflate

: 80704-91-2
(3R,4R)-3,4-bis<(3-methoxyphenyl)methyl>dihydro-2(3H)-furanone

Guidance literature:: With formic acid; 1,3-bis-(diphenylphosphino)propane; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 85 ℃; for 21h;
DOI:10.1021/ol0273598