(1R,3R,8R,9R,10S,11R,12R,14R,19R,20R,21S,22R)-9,10,11,20,21,22-Hexakis-benzyloxy-3,14-bis-(14-hydroxy-tetradecyl)-2,6,13,17,23,24-hexaoxa-tricyclo[17.3.1.1^8,12]tetracosane-5,16-dione

Base Information

• Chemical Name: (1R,3R,8R,9R,10S,11R,12R,14R,19R,20R,21S,22R)-9,10,11,20,21,22-Hexakis-benzyloxy-3,14-bis-(14-hydroxy-tetradecyl)-2,6,13,17,23,24-hexaoxa-tricyclo[17.3.1.1^8,12]tetracosane-5,16-dione
• CAS No.: 465519-09-9
• Molecular Formula: C₈₈H₁₂₀O₁₆
• Molecular Weight: 1433.91

Synonyms:(1R,3R,8R,9R,10S,11R,12R,14R,19R,20R,21S,22R)-9,10,11,20,21,22-Hexakis-benzyloxy-3,14-bis-(14-hydroxy-tetradecyl)-2,6,13,17,23,24-hexaoxa-tricyclo[17.3.1.1^8,12]tetracosane-5,16-dione

Chemical Property of (1R,3R,8R,9R,10S,11R,12R,14R,19R,20R,21S,22R)-9,10,11,20,21,22-Hexakis-benzyloxy-3,14-bis-(14-hydroxy-tetradecyl)-2,6,13,17,23,24-hexaoxa-tricyclo[17.3.1.1^8,12]tetracosane-5,16-dione

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Technology Process of (1R,3R,8R,9R,10S,11R,12R,14R,19R,20R,21S,22R)-9,10,11,20,21,22-Hexakis-benzyloxy-3,14-bis-(14-hydroxy-tetradecyl)-2,6,13,17,23,24-hexaoxa-tricyclo[17.3.1.1^8,12]tetracosane-5,16-dione

There total 1 articles about (1R,3R,8R,9R,10S,11R,12R,14R,19R,20R,21S,22R)-9,10,11,20,21,22-Hexakis-benzyloxy-3,14-bis-(14-hydroxy-tetradecyl)-2,6,13,17,23,24-hexaoxa-tricyclo[17.3.1.1^8,12]tetracosane-5,16-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C120H156O16Si2 (404867-99-8) → (1R,3R,8R,9R,10S,11R,12R,14R,19R,20R,21S,22R)-9,10,11,20,21,22-Hexakis-benzyloxy-3,14-bis-(14-hydroxy-tetradecyl)-2,6,13,17,23,24-hexaoxa-tricyclo[17.3.1.18,12]tetracosane-5,16-dione (465519-09-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1021/ja036521e

Reference yield: 52.0%

tert-butylchlorodiphenylsilane (58479-61-1) + (1R,3R,8R,9R,10S,11R,12R,14R,19R,20R,21S,22R)-9,10,11,20,21,22-Hexakis-benzyloxy-3,14-bis-(14-hydroxy-tetradecyl)-2,6,13,17,23,24-hexaoxa-tricyclo[17.3.1.18,12]tetracosane-5,16-dione (465519-09-9) → (1R,3R,8R,9R,10S,11R,12R,14R,19R,20R,21S,22R)-9,10,11,20,21,22-Hexakis-benzyloxy-14-[14-(tert-butyl-diphenyl-silanyloxy)-tetradecyl]-3-(14-hydroxy-tetradecyl)-2,6,13,17,23,24-hexaoxa-tricyclo[17.3.1.18,12]tetracosane-5,16-dione + C120H156O16Si2 (404867-99-8)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/ja027346p DOI:10.1021/ja036521e

upstream raw materials:

C₁₂₀H₁₅₆O₁₆Si₂

Downstream raw materials:

C₁₂₀H₁₅₆O₁₆Si₂

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