Technology Process of C39H47N7O4
There total 5 articles about C39H47N7O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
1,4-dioxane; water;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium nitrite; sulfuric acid / water / 3 h / 0 °C
1.2: 20 °C
2.1: sodium hydrogencarbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 5 h / 80 °C
3.1: tetrahydrofuran / 1 h / -45 °C
4.1: triethylamine / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 0.5 h / 150 °C / Microwave irradiation
5.1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / Inert atmosphere; Reflux
With
sulfuric acid; sodium hydrogencarbonate; potassium carbonate; triethylamine; sodium nitrite;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water;
2.1: Suzuki Coupling / 5.1: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrahydrofuran / 1 h / -45 °C
2: triethylamine / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 0.5 h / 150 °C / Microwave irradiation
3: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / Inert atmosphere; Reflux
With
potassium carbonate; triethylamine;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; 1,4-dioxane; water;
3: Suzuki Coupling;