1,2,3,4,9,9-Hexachloro-1,4-dihydro-1,4-methanonaphthalene-5,8-diyl diacetate

Base Information

Chemical Name:1,2,3,4,9,9-Hexachloro-1,4-dihydro-1,4-methanonaphthalene-5,8-diyl diacetate
CAS No.:38658-82-1
Molecular Formula:C₁₅H₈Cl₆O₄
Molecular Weight:464.944
Hs Code.:2915390090
DSSTox Substance ID:DTXSID90383591
Nikkaji Number:J814.314E
Mol file:38658-82-1.mol

Synonyms:38658-82-1;1,2,3,4,9,9-Hexachloro-1,4-dihydro-1,4-methanonaphthalene-5,8-diyl diacetate;(6-acetyloxy-1,8,9,10,11,11-hexachloro-3-tricyclo[6.2.1.02,7]undeca-2,4,6,9-tetraenyl) acetate;6-(ACETYLOXY)-1,8,9,10,11,11-HEXACHLOROTRICYCLO[6.2.1.0(2,7)]UNDECA-2,4,6,9-TETRAEN-3-YL ACETATE;SCHEMBL11458832;DTXSID90383591;6-(acetyloxy)-1,8,9,10,11,11-hexachlorotricyclo[6.2.1.0~2,7~]undeca-2,4,6,9-tetraen-3-yl acetate;EU-0001335;FT-0701427;Diacetic acid (5,6,7,8,9,9-hexachloro-5,8-dihydro-5,8-methanonaphthalene)-1,4-diyl ester;6-(acetyloxy)-1,8,9,10,11,11-hexachlorotricyclo[6.2.1.0~2,7~]undeca-2,4,6,9 -tetraen-3-yl acetate

Suppliers and Price of 1,2,3,4,9,9-Hexachloro-1,4-dihydro-1,4-methanonaphthalene-5,8-diyl diacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
6-(ACETYLOXY)-1,8,9,10,11,11-HEXACHLOROTRICYCLO[6.2.1.0(2,7)]UNDECA-2,4,6,9-TETRAEN-3-YL ACETATE 95.00%
5MG
$ 504.31

Total 1 raw suppliers

Chemical Property of 1,2,3,4,9,9-Hexachloro-1,4-dihydro-1,4-methanonaphthalene-5,8-diyl diacetate

Chemical Property:

PSA：52.60000
LogP:5.29570
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:463.852425
Heavy Atom Count:25
Complexity:625

Purity/Quality:: 6-(ACETYLOXY)-1,8,9,10,11,11-HEXACHLOROTRICYCLO[6.2.1.0(2,7)]UNDECA-2,4,6,9-TETRAEN-3-YL ACETATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1=C2C(=C(C=C1)OC(=O)C)C3(C(=C(C2(C3(Cl)Cl)Cl)Cl)Cl)Cl

Technology Process of 1,2,3,4,9,9-Hexachloro-1,4-dihydro-1,4-methanonaphthalene-5,8-diyl diacetate

There total 3 articles about 1,2,3,4,9,9-Hexachloro-1,4-dihydro-1,4-methanonaphthalene-5,8-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.7%

: 101312-35-0
1.2.3.4.9.9-hexachloro-(4arH.8acH)-1.4.4a.8a-tetrahydro-1c.4c-methano-naphthalene-quinone-(5.8)

: 108-24-7
acetic anhydride

: 38658-82-1
1,4-dihydro-5,8-acetoxy-1,2,3,4-tetrachloro-1,4-dichloromethanonaphthalene

Guidance literature:: With pyridine; for 168h; Ambient temperature;
DOI:10.1007/BF01664649

Reference yield:

: 106-51-4
p-benzoquinone

: 38658-82-1
1,4-dihydro-5,8-acetoxy-1,2,3,4-tetrachloro-1,4-dichloromethanonaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / benzene / Heating

2: 65.7 percent / pyridine / 168 h / Ambient temperature

With pyridine; In benzene;
DOI:10.1007/BF01664649

Reference yield:

: 77-47-4
hexachlorocyclopentadiene

: 38658-82-1
1,4-dihydro-5,8-acetoxy-1,2,3,4-tetrachloro-1,4-dichloromethanonaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / benzene / Heating

2: 65.7 percent / pyridine / 168 h / Ambient temperature

With pyridine; In benzene;
DOI:10.1007/BF01664649