3,5-Dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenol

Base Information

Chemical Name:3,5-Dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenol
CAS No.:210833-03-7
Molecular Formula:C₇₆H₇₈O₁₃
Molecular Weight:1199.45
Hs Code.:

Synonyms:3,5-Dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenol

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Chemical Property of 3,5-Dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenol

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Technology Process of 3,5-Dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenol

There total 1 articles about 3,5-Dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 115130-40-0
3,5-dimethoxy-2-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)phenol

: 210833-03-7
3,5-Dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; 1.) - 65 deg C, 30 min; 2.) to RT within 3 h;
DOI:10.1016/S0008-6215(97)10084-2

Reference yield: 87.0%

: 108-24-7
acetic anhydride

: 210833-03-7
3,5-Dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenol

: Acetic acid 3,5-dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenyl ester

Guidance literature:: With dmap; In pyridine; for 12h; Ambient temperature;
DOI:10.1016/S0008-6215(97)10084-2

Reference yield: 81.0%

: 210833-03-7
3,5-Dimethoxy-2,6-bis-((2S,3S,4R,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-phenol

: 210833-04-8
3,5-dimethoxy-2,6-bis(β-D-glucopyranosyl)phenol

Guidance literature:: With hydrogen; palladium on activated charcoal; In 1,4-dioxane; ethanol; acetic acid; for 24h; Ambient temperature;
DOI:10.1016/S0008-6215(97)10084-2