(S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester

Base Information

Chemical Name:(S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester
CAS No.:141437-97-0
Molecular Formula:C₅₂H₅₂N₂O₆S₂
Molecular Weight:865.127
Hs Code.:

(S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester

Synonyms:(S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester

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Chemical Property of (S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester

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MSDS Files:: SDS file from LookChem

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Technology Process of (S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester

There total 9 articles about (S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 962-39-0
L-Phenylalanine benzyl ester

: 141437-87-8
2-(2-Carboxy-3-phenyl-propyldisulfanylmethyl)-3-phenyl-propionic acid

: 141437-97-0
(S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; chloroform; Ambient temperature;
DOI:10.1021/jm00091a016

Reference yield:

: 81110-55-6,69734-01-6
2-mercaptomethyl-3-phenylpropanoic acid

: 141437-97-0
(S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: I₂ / ethanol; H₂O

2: 84 percent / Et₃N, 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / tetrahydrofuran; CHCl₃ / Ambient temperature

With iodine; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform; water;
DOI:10.1021/jm00091a016

Reference yield:

: 91702-98-6,80969-99-9
3-acetylthio-2-benzylpropanoic acid

: 141437-97-0
(S)-2-{2-[2-((S)-1-Benzyloxycarbonyl-2-phenyl-ethylcarbamoyl)-3-phenyl-propyldisulfanylmethyl]-3-phenyl-propionylamino}-3-phenyl-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH / ethanol / 1.5 h / 0 - 20 °C

2: I₂ / ethanol; H₂O

3: 84 percent / Et₃N, 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / tetrahydrofuran; CHCl₃ / Ambient temperature

With sodium hydroxide; iodine; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform; water;
DOI:10.1021/jm00091a016