methyl 2-(2-(3-((2-((tert-butoxycarbonyl)(methyl)amino)ethyl)-(methyl)amino)-3-oxopropyl)phenoxy)acetate

Base Information

• Chemical Name: methyl 2-(2-(3-((2-((tert-butoxycarbonyl)(methyl)amino)ethyl)-(methyl)amino)-3-oxopropyl)phenoxy)acetate
• CAS No.: 1415657-75-8
• Molecular Formula: C₂₁H₃₂N₂O₆
• Molecular Weight: 408.495

Synonyms:methyl 2-(2-(3-((2-((tert-butoxycarbonyl)(methyl)amino)ethyl)-(methyl)amino)-3-oxopropyl)phenoxy)acetate

Chemical Property of methyl 2-(2-(3-((2-((tert-butoxycarbonyl)(methyl)amino)ethyl)-(methyl)amino)-3-oxopropyl)phenoxy)acetate

Chemical Property:

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Technology Process of methyl 2-(2-(3-((2-((tert-butoxycarbonyl)(methyl)amino)ethyl)-(methyl)amino)-3-oxopropyl)phenoxy)acetate

There total 1 articles about methyl 2-(2-(3-((2-((tert-butoxycarbonyl)(methyl)amino)ethyl)-(methyl)amino)-3-oxopropyl)phenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tert-butyl N-methyl-N-<2-(methylamino)ethyl>carbamate (112257-19-9) + C6H4(CH2CH2C(O)O) (119-84-6,1341-36-2) + bromoacetic acid methyl ester (96-32-2) → methyl 2-(2-(3-((2-((tert-butoxycarbonyl)(methyl)amino)ethyl)-(methyl)amino)-3-oxopropyl)phenoxy)acetate (1415657-75-8)

Guidance literature:

tert-butyl N-methyl-N-<2-(methylamino)ethyl>carbamate; C₆H₄(CH₂CH₂C(O)O); In acetonitrile; at 20 ℃; for 16h;

bromoacetic acid methyl ester; With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 2h;

DOI:10.1021/jo302089f

Reference yield:

methyl 2-(2-(3-((2-((tert-butoxycarbonyl)(methyl)amino)ethyl)-(methyl)amino)-3-oxopropyl)phenoxy)acetate (1415657-75-8) → C20H30N2O6

Guidance literature:

With lithium hydroxide monohydrate; In methanol; water; at 20 ℃;

DOI:10.1021/jo302089f

Reference yield:

methyl 2-(2-(3-((2-((tert-butoxycarbonyl)(methyl)amino)ethyl)-(methyl)amino)-3-oxopropyl)phenoxy)acetate (1415657-75-8) → C16H24N2O4

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1.5h;

DOI:10.1021/jo302089f

upstream raw materials:

tert-butyl N-methyl-N-<2-(methylamino)ethyl>carbamate

C₆H₄(CH₂CH₂C(O)O)

bromoacetic acid methyl ester

Downstream raw materials:

tert-butyl (2-(3-(2-(2-((3-hydroxyphenethyl)amino)-2-oxoethoxy)phenyl)-N-methylpropanamido)ethyl)(methyl)carbamate

tert-butyl (2-(3-(2-(2-((2-(1H-imidazol-4-yl)ethyl)amino)-2-oxoethoxy)phenyl)-N-methylpropanamido)ethyl)(methyl)carbamate

3-(2-(2-((3-hydroxyphenethyl)amino)-2-oxoethoxy)phenyl)-N-(2-(2-(2-iodophenyl)-N-methylacetamido)ethyl)-N-methylpropanamide

3-(2-(2-((3-hydroxyphenethyl)amino)-2-oxoethoxy)phenyl)-N-(2-(2-(4-iodophenyl)-N-methylacetamido)ethyl)-N-methylpropanamide

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