1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

Base Information

Chemical Name:1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride
CAS No.:114185-20-5
Molecular Formula:C₂₆H₂₈N₂O₇*ClH
Molecular Weight:516.978
Hs Code.:

Synonyms:1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

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Chemical Property of 1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

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Technology Process of 1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

There total 3 articles about 1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.1%

: 114185-15-8
1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-bis(benzyloxy)-1,2,3,4-tetrahydroisoquinoline

: 114185-20-5
1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; for 4h;
DOI:10.1021/jm00403a006

Reference yield:

: 102921-08-4
1-(3,4,5-trimethoxybenzyl)-6,7-bis(benzyloxy)-1,2,3,4-tetrahydroisoquinoline

: 114185-20-5
1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium bicarbonate, sodium iodide / ethanol / 4 h / Heating

2: 92.1 percent / conc. HCl / methanol / 4 h

With hydrogenchloride; sodium hydrogencarbonate; sodium iodide; In methanol; ethanol;
DOI:10.1021/jm00403a006

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 114185-20-5
1-(3,4,5-trimethoxybenzyl)-2-(4-nitrobenzyl)-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium bicarbonate, sodium iodide / ethanol / 4 h / Heating

2: 92.1 percent / conc. HCl / methanol / 4 h

With hydrogenchloride; sodium hydrogencarbonate; sodium iodide; In methanol; ethanol;
DOI:10.1021/jm00403a006