Technology Process of C14H13FOS
There total 6 articles about C14H13FOS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
at -30 ℃;
for 0.0833333h;
Yield given;
DOI:10.1021/jo00302a052
- Guidance literature:
-
Multi-step reaction with 2 steps
1: (diethylamino)sulfur trifluoride, SbCl3 / CH2Cl2 / 15 min at 0 deg C, then 3 h at room temp.
2: m-chloroperoxybenzoic acid / CHCl3 / 0.08 h / -30 °C
With
diethylamino-sulfur trifluoride; antimony(III) chloride; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; chloroform;
DOI:10.1021/jo00302a052
- Guidance literature:
-
Multi-step reaction with 3 steps
1: m-chloroperoxybenzoic acid (MCPBA) / CHCl3 / 0.08 h / -20 °C
2: (diethylamino)sulfur trifluoride, SbCl3 / CH2Cl2 / 15 min at 0 deg C, then 3 h at room temp.
3: m-chloroperoxybenzoic acid / CHCl3 / 0.08 h / -30 °C
With
diethylamino-sulfur trifluoride; antimony(III) chloride; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; chloroform;
DOI:10.1021/jo00302a052