dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene

Base Information

Chemical Name:dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene
CAS No.:77060-48-1
Molecular Formula:C₁₆H₁₈*2Li
Molecular Weight:224.201
Hs Code.:

Synonyms:dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene

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Chemical Property of dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene

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Technology Process of dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene

There total 3 articles about dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2175-91-9
6,6'-dimethyl fulvene

: 62263-69-8
(lithiomethyl)diphenylphosphane

: 77060-51-6
dilithium salt of 2,4-bis(1,3-cyclopentadienyl)-4-methyl-1-pentene

: 77060-48-1
dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene

: 77061-27-9
lithium <1,1-dimethyl-2-(diphenylphosphino)ethyl>cyclopentadienide

: 1486-28-8
diphenyl(methyl)phosphine

Guidance literature:: In Petroleum ether; at 27 ℃; for 168h;
DOI:10.1021/jo00324a019

Reference yield: 78.0%

: 2175-91-9
6,6'-dimethyl fulvene

: 62263-69-8
(lithiomethyl)diphenylphosphane

: 77060-52-7
lithium (1-methylethenyl)cyclopentadiene

: 77060-51-6
dilithium salt of 2,4-bis(1,3-cyclopentadienyl)-4-methyl-1-pentene

: 77060-48-1
dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene

: 77061-27-9
lithium <1,1-dimethyl-2-(diphenylphosphino)ethyl>cyclopentadienide

: 1486-28-8
diphenyl(methyl)phosphine

Guidance literature:: In Petroleum ether; at 27 ℃; for 168h; Product distribution;
DOI:10.1021/jo00324a019

Reference yield:

: 2175-91-9
6,6'-dimethyl fulvene

: 77060-52-7
lithium (1-methylethenyl)cyclopentadiene

: 77060-51-6
dilithium salt of 2,4-bis(1,3-cyclopentadienyl)-4-methyl-1-pentene

: 77060-48-1
dilithium salt of 6-(1,3-cyclopentadienyl)-6,8,8-trimethylbicyclo<3.3.0>octa-1,3-diene

: 77061-27-9
lithium <1,1-dimethyl-2-(diphenylphosphino)ethyl>cyclopentadienide

Guidance literature:: With (lithiomethyl)diphenylphosphane; In Petroleum ether; at 27 ℃; for 7h; Further byproducts given. Yields of byproduct given;
DOI:10.1021/jo00324a019