1,3-bis(2′,6′-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene

Base Information

• Chemical Name: 1,3-bis(2′,6′-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene
• CAS No.: 1034137-54-6
• Molecular Formula: C₂₉H₄₂N₂
• Molecular Weight: 418.666

Synonyms:1,3-bis(2′,6′-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene

Chemical Property of 1,3-bis(2′,6′-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene

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Technology Process of 1,3-bis(2′,6′-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene

There total 8 articles about 1,3-bis(2′,6′-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF4 (1034137-39-7) + 1,3-bis(2,6-diisopropylphenyl)tetrahydropyrimidin-2-ylidene (1034137-51-3) → (1,3-bis(2,6-diisopropylphenyl)-3,4,5,6-tetrahydropyrimidin-1-ium)BF4 (1034137-33-1) + 1,3-bis(2′,6′-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene (1034137-54-6)

Guidance literature:

In benzene-d6; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/anie.202111588

Reference yield:

1-(2,6-diisopropylphenyl)-3,3,5,5-tetramethylpyrrolidin-2-ylidene + (1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF4 (1034137-39-7) → 1,3-bis(2′,6′-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene (1034137-54-6) + C20H32N(1+)*BF4(1-)

Guidance literature:

In benzene-d6; at 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1002/anie.202111588

Reference yield:

(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF4 (1034137-39-7) + C24H37N → 1,3-bis(2′,6′-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene (1034137-54-6) + C24H38N(1+)*BF4(1-)

Guidance literature:

In benzene-d6; at 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1002/anie.202111588

upstream raw materials:

(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄

2,6-diisopropylbenzenamine

N,N'-di(2,6-diisopropylphenyl)formamidine

1,3-bis(2,6-diisopropylphenyl)tetrahydropyrimidin-2-ylidene

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