1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-manno-hept-1-enitol

Base Information

Chemical Name:1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-manno-hept-1-enitol
CAS No.:105539-44-4
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:

Synonyms:1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-manno-hept-1-enitol

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Chemical Property of 1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-manno-hept-1-enitol

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Technology Process of 1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-manno-hept-1-enitol

There total 3 articles about 1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-manno-hept-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 89363-64-4,105926-77-0
(+/-)-<2α(R*),3α>-2,3-dihydro-3,5-dimethyl-2-<1-methyl-2-(phenylmethoxy)ethyl>-4H-pyran-4-one

: 105539-44-4
1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-manno-hept-1-enitol

: 105581-62-2
1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-gluco-3-heptulose

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -78 ℃;
DOI:10.1021/ja00237a037

Reference yield:

: 72486-93-2
1-methoxy-2-methyl-3-trimethylsiloxy-1,3-pentadiene

: 105539-44-4
1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-manno-hept-1-enitol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) TiCl₄ / 1) CH₂Cl₂, -78 deg C, 5 min, 2) CH₂Cl₂, -78 deg C, 30 min

2: 91 percent / LiAlH₄ / diethyl ether / -78 °C

With lithium aluminium tetrahydride; titanium tetrachloride; In diethyl ether;
DOI:10.1021/ja00237a037

Reference yield:

: 74130-31-7,79026-61-2,79027-28-4,73814-73-0
3-(benzyloxy)-2-methylpropanal

: 105539-44-4
1,5-anhydro-2,4,6-trideoxy-2,4,6-trimethyl-7-O-(phenylmethyl)-DL-manno-hept-1-enitol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) TiCl₄ / 1) CH₂Cl₂, -78 deg C, 5 min, 2) CH₂Cl₂, -78 deg C, 30 min

2: 91 percent / LiAlH₄ / diethyl ether / -78 °C

With lithium aluminium tetrahydride; titanium tetrachloride; In diethyl ether;
DOI:10.1021/ja00237a037