C₂₀H₂₈O₃Si

Base Information

Chemical Name:C₂₀H₂₈O₃Si
CAS No.:902132-27-8
Molecular Formula:C₂₀H₂₈O₃Si
Molecular Weight:344.526
Hs Code.:

C<sub>20</sub>H<sub>28</sub>O<sub>3</sub>Si

Synonyms:C₂₀H₂₈O₃Si

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Chemical Property of C₂₀H₂₈O₃Si

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Technology Process of C₂₀H₂₈O₃Si

There total 3 articles about C₂₀H₂₈O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 902132-15-4
C₂₀H₃₀O₃Si

: 902132-27-8
C₂₀H₂₈O₃Si

Guidance literature:: With ortho-iodoxybenzoic acid; In dimethyl sulfoxide; at 25 ℃; for 2h;
DOI:10.1039/b602020h

Reference yield:

: 902132-11-0
(3R,4S)-3-(4-methoxybenzyloxy)-4-methyl-5-hexenal

: 902132-27-8
C₂₀H₂₈O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C

1.2: tetrahydrofuran; hexane / 2 h / -78 - 0 °C

2.1: 78 percent / ortho-iodoxybenzoic acid / dimethylsulfoxide / 2 h / 25 °C

With n-butyllithium; ortho-iodoxybenzoic acid; In tetrahydrofuran; hexane; dimethyl sulfoxide;
DOI:10.1039/b602020h

Reference yield:

: 259656-95-6
(3R,4S)-3-(4-methoxybenzyloxy)-4-methyl-5-hexen-1-ol

: 902132-27-8
C₂₀H₂₈O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 96 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 1 h / -78 - 25 °C

2.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C

2.2: tetrahydrofuran; hexane / 2 h / -78 - 0 °C

3.1: 78 percent / ortho-iodoxybenzoic acid / dimethylsulfoxide / 2 h / 25 °C

With n-butyllithium; oxalyl dichloride; ortho-iodoxybenzoic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; 1.1: Swern oxidation;
DOI:10.1039/b602020h