ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate

Base Information

Chemical Name:ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate
CAS No.:1361152-02-4
Molecular Formula:C₃₇H₂₆F₃O₅PS
Molecular Weight:670.645
Hs Code.:

Synonyms:ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate

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Chemical Property of ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate

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Technology Process of ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate

There total 1 articles about ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1344732-82-6
(methoxymethyl)phenylphosphine oxide

: 157397-72-3,221694-49-1
rac-[4,4'-biphenanthrene]-3,3'-diyl bis-trifluoromethanesulfonate

: 1361152-02-4
ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate

Guidance literature:: With sodium formate; palladium diacetate; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; In dimethyl sulfoxide; at 110 ℃; for 57h; Inert atmosphere;
DOI:10.1002/anie.201106157

Reference yield: 34.0%

: 1361152-02-4
ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate

: 1361152-00-2,1361191-95-8,1361192-28-0
9-phenylnaphtho[1,2-e]phenanthro[3,4-b]phosphindole 9-oxide

Guidance literature:: ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate; With lithium aluminium tetrahydride; chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 20 ℃; for 20h; Inert atmosphere;

With palladium diacetate; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; In dimethyl sulfoxide; at 110 ℃; for 16h; Inert atmosphere;

With dihydrogen peroxide; In dichloromethane; water; dimethyl sulfoxide; at 20 ℃; for 12h;
DOI:10.1002/anie.201106157

Reference yield:

: 1361152-02-4
ethyl phenyl(3'-trifluoromethanesulfonyloxy-4,4'-biphenanthryl-3-ly)phosphinate

: 1361152-03-5
C₃₅H₂₂F₃O₃PS

Guidance literature:: With lithium aluminium tetrahydride; chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 20 ℃; for 20h; Inert atmosphere;
DOI:10.1002/anie.201106157