(1R,2R)-N,N′-bis[(5-methylfuran-2-yl)methylidene]cyclohexane-1,2-diamine

Base Information

• Chemical Name: (1R,2R)-N,N′-bis[(5-methylfuran-2-yl)methylidene]cyclohexane-1,2-diamine
• CAS No.: 1598408-94-6
• Molecular Formula: C₁₈H₂₂N₂O₂
• Molecular Weight: 298.385

Synonyms:(1R,2R)-N,N′-bis[(5-methylfuran-2-yl)methylidene]cyclohexane-1,2-diamine

Chemical Property of (1R,2R)-N,N′-bis[(5-methylfuran-2-yl)methylidene]cyclohexane-1,2-diamine

Chemical Property:

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Technology Process of (1R,2R)-N,N′-bis[(5-methylfuran-2-yl)methylidene]cyclohexane-1,2-diamine

There total 2 articles about (1R,2R)-N,N′-bis[(5-methylfuran-2-yl)methylidene]cyclohexane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

5-Methylfurfural (620-02-0) + (1R,2R)-(-)-1,2-diammoniumcyclohexane mono-L-(+)-tartrate (116407-32-0,32044-22-7,39961-95-0) → (1R,2R)-N,N′-bis[(5-methylfuran-2-yl)methylidene]cyclohexane-1,2-diamine (1598408-94-6)

Guidance literature:

With sodium hydroxide; In dichloromethane; water; at 20 ℃; for 72h;

DOI:10.1016/j.ica.2018.04.025

Reference yield: 90.0%

5-Methylfurfural (620-02-0) + (1R,2R)-1,2-diaminocyclohexane tartrate (32044-22-7,39961-95-0) → (1R,2R)-N,N′-bis[(5-methylfuran-2-yl)methylidene]cyclohexane-1,2-diamine (1598408-94-6)

Guidance literature:

With potassium carbonate; In ethanol; at 40 - 45 ℃; for 1.08333h; Irradiation;

DOI:10.1016/j.tet.2014.02.092

Reference yield: 94.0%

(1R,2R)-N,N′-bis[(5-methylfuran-2-yl)methylidene]cyclohexane-1,2-diamine (1598408-94-6) → (R,R)-N1,N2-bis((5-methylfuran-2-yl)methyl)cyclohexane-1,2-diamine (1598408-97-9)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 1h; Reflux;

DOI:10.1016/j.tet.2014.02.092

upstream raw materials:

5-Methylfurfural

(1R,2R)-1,2-diaminocyclohexane tartrate

(1R,2R)-(-)-1,2-diammoniumcyclohexane mono-L-(+)-tartrate

Downstream raw materials:

(R,R)-N¹,N²-bis((5-methylfuran-2-yl)methyl)cyclohexane-1,2-diamine

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