5,5'-(5,5'-(5-tert-butyl-1,3-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene)bis(3-tert-butyl-5,1-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene))bis(3-tert-butyl-5,1-phenylene)dimethanethiol

Base Information

• Chemical Name: 5,5'-(5,5'-(5-tert-butyl-1,3-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene)bis(3-tert-butyl-5,1-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene))bis(3-tert-butyl-5,1-phenylene)dimethanethiol
• CAS No.: 1056547-95-5
• Molecular Formula: C₆₀H₈₂S₆
• Molecular Weight: 995.707

Synonyms:5,5'-(5,5'-(5-tert-butyl-1,3-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene)bis(3-tert-butyl-5,1-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene))bis(3-tert-butyl-5,1-phenylene)dimethanethiol

Chemical Property of 5,5'-(5,5'-(5-tert-butyl-1,3-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene)bis(3-tert-butyl-5,1-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene))bis(3-tert-butyl-5,1-phenylene)dimethanethiol

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Technology Process of 5,5'-(5,5'-(5-tert-butyl-1,3-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene)bis(3-tert-butyl-5,1-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene))bis(3-tert-butyl-5,1-phenylene)dimethanethiol

There total 1 articles about 5,5'-(5,5'-(5-tert-butyl-1,3-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene)bis(3-tert-butyl-5,1-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene))bis(3-tert-butyl-5,1-phenylene)dimethanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(5-tert-butyl-1,3-phenylene)bis(methylene)bis((3-tert-butyl-5-((3-tert-butyl-5-(tritylthiomethyl)benzylthio)methyl)benzyl)sulfane) (1056547-94-4) → 5,5'-(5,5'-(5-tert-butyl-1,3-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene)bis(3-tert-butyl-5,1-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene))bis(3-tert-butyl-5,1-phenylene)dimethanethiol (1056547-95-5)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.25h;

DOI:10.1039/b802460j

Reference yield: 99.0%

5,5'-(5,5'-(5-tert-butyl-1,3-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene)bis(3-tert-butyl-5,1-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene))bis(3-tert-butyl-5,1-phenylene)dimethanethiol (1056547-95-5) + benzyl chloride (100-44-7) → (5-tert-butyl-1,3-phenylene)bis(methylene)bis((3-((3-(benzylthiomethyl)-5-tert-butylbenzylthio)methyl)-5-tert-butylbenzyl)sulfane) (1056547-89-7)

Guidance literature:

With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1039/b802460j

Reference yield: 92.0%

(3-(bromomethyl)-5-tert-butylbenzyl)(trityl)sulfane (1056547-91-1) + 5,5'-(5,5'-(5-tert-butyl-1,3-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene)bis(3-tert-butyl-5,1-phenylene)bis(methylene)bis(sulfanediyl)bis(methylene))bis(3-tert-butyl-5,1-phenylene)dimethanethiol (1056547-95-5) → (5-tert-butyl-1,3-phenylene)bis(methylene)bis((3-tert-butyl-5-((3-tert-butyl-5-((3-tert-butyl-5-(tritylthiomethyl)benzylthio)methyl)benzylthio)methyl)benzyl)sulfane) (1056547-96-6)

Guidance literature:

With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1039/b802460j

upstream raw materials:

(5-tert-butyl-1,3-phenylene)bis(methylene)bis((3-tert-butyl-5-((3-tert-butyl-5-(tritylthiomethyl)benzylthio)methyl)benzyl)sulfane)

Downstream raw materials:

(5-tert-butyl-1,3-phenylene)bis(methylene)bis((3-tert-butyl-5-((3-tert-butyl-5-((3-tert-butyl-5-(tritylthiomethyl)benzylthio)methyl)benzylthio)methyl)benzyl)sulfane)

(5-tert-butyl-1,3-phenylene)bis(methylene)bis((3-((3-(benzylthiomethyl)-5-tert-butylbenzylthio)methyl)-5-tert-butylbenzyl)sulfane)

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