(E)-2-(chloromethyl)-4-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide

Base Information

Chemical Name:(E)-2-(chloromethyl)-4-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide
CAS No.:1381789-17-8
Molecular Formula:C₂₉H₃₈ClNO₄
Molecular Weight:500.078
Hs Code.:

Synonyms:(E)-2-(chloromethyl)-4-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide

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Chemical Property of (E)-2-(chloromethyl)-4-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide

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Technology Process of (E)-2-(chloromethyl)-4-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide

There total 4 articles about (E)-2-(chloromethyl)-4-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1381789-16-7
(E)-4-(3,7-dimethylocta-2,6-dienyl)-2-(hydroxymethyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide

: 1381789-17-8
(E)-2-(chloromethyl)-4-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/jo300719m

Reference yield:

: 1345545-23-4
(E)-6-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-7-(methoxymethoxy)isobenzofuran-1(3H)-one

: 1381789-17-8
(E)-2-(chloromethyl)-4-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

2.1: silver carbonate / toluene / 1 h / Reflux

3.1: trimethylaluminum / hexane; 1,2-dichloro-ethane / 0.5 h / 20 °C

3.2: 7.5 h / 40 °C

4.1: methanesulfonyl chloride; triethylamine / dichloromethane / 2 h / 0 °C

With lithium aluminium tetrahydride; trimethylaluminum; methanesulfonyl chloride; triethylamine; silver carbonate; In tetrahydrofuran; hexane; dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.1021/jo300719m

Reference yield:

: 1345545-24-5
C₂₁H₃₂O₅

: 1381789-17-8
(E)-2-(chloromethyl)-4-(3,7-dimethylocta-2,6-dienyl)-5-methoxy-3-(methoxymethoxy)-N-phenethylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: silver carbonate / toluene / 1 h / Reflux

2.1: trimethylaluminum / hexane; 1,2-dichloro-ethane / 0.5 h / 20 °C

2.2: 7.5 h / 40 °C

3.1: methanesulfonyl chloride; triethylamine / dichloromethane / 2 h / 0 °C

With trimethylaluminum; methanesulfonyl chloride; triethylamine; silver carbonate; In hexane; dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.1021/jo300719m