1,3,2-Dioxathiolane,4-(1-methylethyl)-,2,2-dioxide,(4R)-(9CI)

Base Information

• Chemical Name: 1,3,2-Dioxathiolane,4-(1-methylethyl)-,2,2-dioxide,(4R)-(9CI)
• CAS No.: 291780-07-9
• Molecular Formula: C₅H₁₀O₄S
• Molecular Weight: 166.198
• Mol file: 291780-07-9.mol

Synonyms:1,3,2-Dioxathiolane,4-(1-methylethyl)-,2,2-dioxide,(4R)-(9CI)

Chemical Property of 1,3,2-Dioxathiolane,4-(1-methylethyl)-,2,2-dioxide,(4R)-(9CI)

Chemical Property:

• PSA: 60.98000
• LogP: 1.38340

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1,3,2-Dioxathiolane,4-(1-methylethyl)-,2,2-dioxide,(4R)-(9CI)

There total 3 articles about 1,3,2-Dioxathiolane,4-(1-methylethyl)-,2,2-dioxide,(4R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-4-Isopropyl-[1,3,2]dioxathiolane 2-oxide → (S)-4-Isopropyl-[1,3,2]dioxathiolane 2,2-dioxide (168141-49-9,176094-53-4,291780-07-9)

Guidance literature:

With ruthenium trichloride; sodium periodate; In water; acetonitrile; at 25 ℃;

DOI:10.1016/0040-4039(95)00382-M

Reference yield:

4-Isopropyl-[1,3,2]dioxathiolane 2-oxide → 4-(1-methylethyl)-1,3,2-dioxathiolane 2,2-dioxide (176094-53-4,291780-07-9)

Guidance literature:

With ruthenium(IV) oxide; sodium periodate; In dichloromethane; water; acetonitrile; at 20 ℃; for 24h; Yield given;

DOI:10.1055/s-1996-4193

Reference yield:

3-methylbutane-1,2-diol (50468-22-9) → 4-(1-methylethyl)-1,3,2-dioxathiolane 2,2-dioxide (176094-53-4,291780-07-9)

Guidance literature:

Multi-step reaction with 2 steps

1: NEt₃, SOCl₂ / diethyl ether; CH₂Cl₂ / 2 h / 20 °C

2: NaIO₄, RuO₂ / CH₂Cl₂; acetonitrile; H₂O / 24 h / 20 °C

With ruthenium(IV) oxide; sodium periodate; thionyl chloride; triethylamine; In diethyl ether; dichloromethane; water; acetonitrile;

DOI:10.1055/s-1996-4193

upstream raw materials:

3-methylbutane-1,2-diol

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