1-nitro-2-phenyl-2-propargyloxyethane

Base Information

Chemical Name:1-nitro-2-phenyl-2-propargyloxyethane
CAS No.:157024-32-3
Molecular Formula:C₁₁H₁₁NO₃
Molecular Weight:205.213
Hs Code.:

Synonyms:1-nitro-2-phenyl-2-propargyloxyethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-nitro-2-phenyl-2-propargyloxyethane

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Technology Process of 1-nitro-2-phenyl-2-propargyloxyethane

There total 2 articles about 1-nitro-2-phenyl-2-propargyloxyethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 5153-67-3
nitrostyrene

: 107-19-7
propargyl alcohol

: 157024-32-3
1-nitro-2-phenyl-2-propargyloxyethane

: 2-phenyl-2-propargyloxyethanohydroximoyl chloride

Guidance literature:: nitrostyrene; propargyl alcohol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 3h;

With hydrogenchloride; In tetrahydrofuran; for 0.5h; ice cooling;
DOI:10.1016/S0040-4020(98)00883-7

Reference yield: 66.0%

: 102-96-5
(2-nitroethenyl)benzene

: 107-19-7
propargyl alcohol

: 157024-32-3
1-nitro-2-phenyl-2-propargyloxyethane

Guidance literature:: propargyl alcohol; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere;

(2-nitroethenyl)benzene; In tetrahydrofuran; hexane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2011.12.010