1-(4-(bromodifluoromethyl)-3,5-difluorophenyl)-4-propyl-2,6,7-trioxabicyclo[2.2.2]octane

Base Information

Chemical Name:1-(4-(bromodifluoromethyl)-3,5-difluorophenyl)-4-propyl-2,6,7-trioxabicyclo[2.2.2]octane
CAS No.:1401904-34-4
Molecular Formula:C₁₅H₁₅BrF₄O₃
Molecular Weight:399.18
Hs Code.:

Synonyms:1-(4-(bromodifluoromethyl)-3,5-difluorophenyl)-4-propyl-2,6,7-trioxabicyclo[2.2.2]octane

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Chemical Property of 1-(4-(bromodifluoromethyl)-3,5-difluorophenyl)-4-propyl-2,6,7-trioxabicyclo[2.2.2]octane

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Technology Process of 1-(4-(bromodifluoromethyl)-3,5-difluorophenyl)-4-propyl-2,6,7-trioxabicyclo[2.2.2]octane

There total 6 articles about 1-(4-(bromodifluoromethyl)-3,5-difluorophenyl)-4-propyl-2,6,7-trioxabicyclo[2.2.2]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-61-6
dibromodifluoromethane

: 1401904-32-2
4-propyl-1-(3,5-difluorophenyl)-2,6,7-trioxabicyclo[2.2.2]octane

: 1401904-34-4
1-(4-(bromodifluoromethyl)-3,5-difluorophenyl)-4-propyl-2,6,7-trioxabicyclo[2.2.2]octane

Guidance literature:: dibromodifluoromethane; 4-propyl-1-(3,5-difluorophenyl)-2,6,7-trioxabicyclo[2.2.2]octane; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; for 1h; Inert atmosphere;

With dibromodifluoromethane; In tetrahydrofuran; hexane; at -70 ℃; for 1h; Inert atmosphere;

Reference yield:

: 7426-71-3
2-(hydroxymethyl)-2-propylpropane-1,3-diol

: 1401904-34-4
1-(4-(bromodifluoromethyl)-3,5-difluorophenyl)-4-propyl-2,6,7-trioxabicyclo[2.2.2]octane

Guidance literature:: Multi-step reaction with 4 steps

1.1: Diethyl carbonate; potassium carbonate / 6 h / 125 °C / Inert atmosphere

2.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 24 h / -70 - 20 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -70 °C / Inert atmosphere

4.2: 1 h / -70 °C / Inert atmosphere

With dmap; n-butyllithium; boron trifluoride diethyl etherate; potassium carbonate; dicyclohexyl-carbodiimide; Diethyl carbonate; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 107829-94-7
3-hydroxymethyl-3-n-propyl oxetane

: 1401904-34-4
1-(4-(bromodifluoromethyl)-3,5-difluorophenyl)-4-propyl-2,6,7-trioxabicyclo[2.2.2]octane

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 24 h / -70 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -70 °C / Inert atmosphere

3.2: 1 h / -70 °C / Inert atmosphere

With dmap; n-butyllithium; boron trifluoride diethyl etherate; dicyclohexyl-carbodiimide; In tetrahydrofuran; hexane; dichloromethane;