α-allyl-α-benzoyldithioacetate

Base Information

Chemical Name:α-allyl-α-benzoyldithioacetate
CAS No.:97510-22-0
Molecular Formula:C₁₃H₁₄OS₂
Molecular Weight:250.386
Hs Code.:

Synonyms:α-allyl-α-benzoyldithioacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-allyl-α-benzoyldithioacetate

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Technology Process of α-allyl-α-benzoyldithioacetate

There total 1 articles about α-allyl-α-benzoyldithioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 13636-68-5
methyl 3-hydroxy-3-phenylprop-2-enedithioate

: 106-95-6
allyl bromide

: 97510-22-0
α-allyl-α-benzoyldithioacetate

Guidance literature:: With indium; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Solvent; Temperature; Reagent/catalyst;
DOI:10.1002/ejoc.201301788

Reference yield: 87.0%

: 97510-22-0
α-allyl-α-benzoyldithioacetate

: 3-benzoyl-2-(methylthio)-4H-thiopyran

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; triphenylphosphine; In toluene; at 100 ℃; for 12h; Solvent; Temperature; Reagent/catalyst; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol502850h

Reference yield: 83.0%

: 97510-22-0
α-allyl-α-benzoyldithioacetate

: 3-benzoyl-5-methyl-2-(methylthio)-4,5-dihydrothiophene

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 12h; Solvent; Reagent/catalyst; regioselective reaction; Catalytic behavior; Inert atmosphere;
DOI:10.1021/ol502850h