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Technology Process of N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine

N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine

Base Information
  • Chemical Name:N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine
  • CAS No.:108017-73-8
  • Molecular Formula:C28H35N5O9
  • Molecular Weight:585.614
  • Hs Code.:
<i>N</i><sup>6</sup>-benzyloxycarbonyl-<i>N</i><sup>2</sup>-{<i>N</i>-[<i>N</i>-(<i>N</i>-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine

Synonyms:N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine

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Chemical Property of N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine
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Technology Process of N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine

There total 2 articles about N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

CbzGlyGly
2566-19-0

CbzGlyGly

<i>N</i><sup>6</sup>-benzyloxycarbonyl-<i>N</i><sup>2</sup>-{<i>N</i>-[<i>N</i>-(<i>N</i>-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine
108017-73-8

N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine

Guidance literature:
Multi-step reaction with 2 steps
1: chlorocarbonic acid isobutyl ester; triethylamine; THF / anschliessend Behandeln mit N6-Benzyloxycarbonyl-N2-glycyl-L-lysin-methylester-hydrochlorid und Triaethylamin in CHCl3
2: methanol; aqueous NaOH
With tetrahydrofuran; methanol; sodium hydroxide; triethylamine; isobutyl chloroformate;

Reference yield:

<i>N</i><sup>6</sup>-benzyloxycarbonyl-<i>N</i><sup>2</sup>-{<i>N</i>-[<i>N</i>-(<i>N</i>-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine methyl ester
116929-50-1

N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine methyl ester

<i>N</i><sup>6</sup>-benzyloxycarbonyl-<i>N</i><sup>2</sup>-{<i>N</i>-[<i>N</i>-(<i>N</i>-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine
108017-73-8

N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine

Guidance literature:
With methanol; sodium hydroxide;
upstream raw materials:

N6-benzyloxycarbonyl-N2-{N-[N-(N-benzyloxycarbonyl-glycyl)-glycyl]-glycyl}-L-lysine methyl ester

CbzGlyGly

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