N,N'-bis(N-benzyloxycarbonyl)-1,24-diamino-4,21-dioxa-5,20-dioxotetracosane

Base Information

Chemical Name:N,N'-bis(N-benzyloxycarbonyl)-1,24-diamino-4,21-dioxa-5,20-dioxotetracosane
CAS No.:217471-34-6
Molecular Formula:C₃₈H₅₆N₂O₈
Molecular Weight:668.871
Hs Code.:

Synonyms:N,N'-bis(N-benzyloxycarbonyl)-1,24-diamino-4,21-dioxa-5,20-dioxotetracosane

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Chemical Property of N,N'-bis(N-benzyloxycarbonyl)-1,24-diamino-4,21-dioxa-5,20-dioxotetracosane

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Technology Process of N,N'-bis(N-benzyloxycarbonyl)-1,24-diamino-4,21-dioxa-5,20-dioxotetracosane

There total 2 articles about N,N'-bis(N-benzyloxycarbonyl)-1,24-diamino-4,21-dioxa-5,20-dioxotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 34959-19-8
1,16-hexadecanedioyl dichloride

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 217471-34-6
N,N'-bis(N-benzyloxycarbonyl)-1,24-diamino-4,21-dioxa-5,20-dioxotetracosane

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jo981195k

Reference yield:

: 505-54-4
thapsic acid

: 217471-34-6
N,N'-bis(N-benzyloxycarbonyl)-1,24-diamino-4,21-dioxa-5,20-dioxotetracosane

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 3 h / Heating

2: 58 percent / DMAP / CH₂Cl₂ / 24 h / 20 °C

With dmap; thionyl chloride; In dichloromethane; 1: Substitution / 2: Esterification;
DOI:10.1021/jo981195k