N,N',N''-tris[acetic acid 2-acetoxy-1-{5-[(2,3-dihydroxypropyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester benzoyl]-1,5,10-triazadecane

Base Information

• Chemical Name: N,N',N''-tris[acetic acid 2-acetoxy-1-{5-[(2,3-dihydroxypropyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester benzoyl]-1,5,10-triazadecane
• CAS No.: 1097772-75-2
• Molecular Formula: C₆₄H₇₆I₉N₉O₂₇
• Molecular Weight: 2545.49

Synonyms:N,N',N''-tris[acetic acid 2-acetoxy-1-{5-[(2,3-dihydroxypropyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester benzoyl]-1,5,10-triazadecane

Chemical Property of N,N',N''-tris[acetic acid 2-acetoxy-1-{5-[(2,3-dihydroxypropyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester benzoyl]-1,5,10-triazadecane

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Technology Process of N,N',N''-tris[acetic acid 2-acetoxy-1-{5-[(2,3-dihydroxypropyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester benzoyl]-1,5,10-triazadecane

There total 1 articles about N,N',N''-tris[acetic acid 2-acetoxy-1-{5-[(2,3-dihydroxypropyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester benzoyl]-1,5,10-triazadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic acid 2-acetoxy-1-{3-chlorocarbonyl-5-[(2,3-dihydroxy-propyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester (1097772-73-0) + N-(3-aminopropyl)-1,4-diaminobutane (124-20-9) → N,N',N''-tris[acetic acid 2-acetoxy-1-{5-[(2,3-dihydroxypropyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester benzoyl]-1,5,10-triazadecane (1097772-75-2)

Guidance literature:

With triethylamine; In N,N-dimethyl acetamide; at 20 ℃; for 24h;

Reference yield:

N,N',N''-tris[acetic acid 2-acetoxy-1-{5-[(2,3-dihydroxypropyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester benzoyl]-1,5,10-triazadecane (1097772-75-2) → N-[3-(N-(2,3-dihydroxypropyl)-5-(2,3-dihydroxy-propionylamino)-N-methyl-2,4,6-triiodo-isophthalylamino)-propyl]-N-[4-(N-(2,3-dihydroxypropyl)-5-(2,3-dihydroxy-propionylamino)-N-methyl-2,4,6-triiodo-isophthalylamino)-butyl]-N'-(2,3-dihydroxy-propyl)-5-(2,3-dihydroxy-propionylamino)-N'-methyl-2,4,6-triiodo-isophthalamide (1097772-05-8)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 24h;

upstream raw materials:

acetic acid 2-acetoxy-1-{3-chlorocarbonyl-5-[(2,3-dihydroxy-propyl)-methyl-carbamoyl]-2,4,6-triiodo-phenylcarbamoyl}-ethyl ester

N-(3-aminopropyl)-1,4-diaminobutane

Downstream raw materials:

N-[3-(N-(2,3-dihydroxypropyl)-5-(2,3-dihydroxy-propionylamino)-N-methyl-2,4,6-triiodo-isophthalylamino)-propyl]-N-[4-(N-(2,3-dihydroxypropyl)-5-(2,3-dihydroxy-propionylamino)-N-methyl-2,4,6-triiodo-isophthalylamino)-butyl]-N'-(2,3-dihydroxy-propyl)-5-(2,3-dihydroxy-propionylamino)-N'-methyl-2,4,6-triiodo-isophthalamide

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