9-Biphenyl-2-ylthioxanthene

Base Information

• Chemical Name: 9-Biphenyl-2-ylthioxanthene
• CAS No.: 118385-22-1
• Molecular Formula: C₂₅H₁₈S
• Molecular Weight: 350.484

Synonyms:9-Biphenyl-2-ylthioxanthene

Chemical Property of 9-Biphenyl-2-ylthioxanthene

Chemical Property:

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Technology Process of 9-Biphenyl-2-ylthioxanthene

There total 1 articles about 9-Biphenyl-2-ylthioxanthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Bromobiphenyl (2052-07-5) + Thioxanthylium perchlorate (2567-20-6) → 9-Biphenyl-2-ylthioxanthene (118385-22-1)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1.) ether, 2.) ether, 15, reflux;

Reference yield: 81.0%

9-Biphenyl-2-ylthioxanthene (118385-22-1) → 9-Biphenyl-2-ylthioxanthene 10-oxide (118404-01-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 24h;

Reference yield: 80.0%

diphenyliodonium tetrafluoroborate + 9-Biphenyl-2-ylthioxanthene (118385-22-1) → C31H23S(1+)*BF4(1-)

Guidance literature:

With copper(II) benzoate; In various solvent(s); at 125 - 135 ℃; for 5h;

upstream raw materials:

2-Bromobiphenyl

Thioxanthylium perchlorate

Downstream raw materials:

9-Biphenyl-2-ylthioxanthene 10-oxide

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