2-(3',4'-Dimethoxy-β-phenethyl)-6,7-methylenedioxy-1,2,3,4-tetrahydro-3-isoquinolone

Base Information

Chemical Name:2-(3',4'-Dimethoxy-β-phenethyl)-6,7-methylenedioxy-1,2,3,4-tetrahydro-3-isoquinolone
CAS No.:72584-21-5
Molecular Formula:C₂₀H₂₁NO₅
Molecular Weight:355.39
Hs Code.:

Synonyms:2-(3',4'-Dimethoxy-β-phenethyl)-6,7-methylenedioxy-1,2,3,4-tetrahydro-3-isoquinolone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3',4'-Dimethoxy-β-phenethyl)-6,7-methylenedioxy-1,2,3,4-tetrahydro-3-isoquinolone

Chemical Property:

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Technology Process of 2-(3',4'-Dimethoxy-β-phenethyl)-6,7-methylenedioxy-1,2,3,4-tetrahydro-3-isoquinolone

There total 4 articles about 2-(3',4'-Dimethoxy-β-phenethyl)-6,7-methylenedioxy-1,2,3,4-tetrahydro-3-isoquinolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 72600-39-6
ethyl 2-bromomethyl-4,5-methylenedioxyphenyl acetate

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 72584-21-5
2-(3',4'-Dimethoxy-β-phenethyl)-6,7-methylenedioxy-1,2,3,4-tetrahydro-3-isoquinolone

Guidance literature:: With potassium carbonate; potassium iodide; In ethanol; Heating;

Reference yield:

: 34140-20-0
6,7-(methylenedioxy)isochroman-3-one

: 72584-21-5
2-(3',4'-Dimethoxy-β-phenethyl)-6,7-methylenedioxy-1,2,3,4-tetrahydro-3-isoquinolone

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / HBr / ethanol / 24 h / Ambient temperature

2: 78 percent / K₂CO₃/KI / ethanol / Heating

With hydrogen bromide; potassium carbonate; potassium iodide; In ethanol;

Reference yield:

: 4230-93-7
1,2-dimethoxy-4-(2-nitro-vinyl)-benzene

: 72584-21-5
2-(3',4'-Dimethoxy-β-phenethyl)-6,7-methylenedioxy-1,2,3,4-tetrahydro-3-isoquinolone

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄

2: 78 percent / K₂CO₃/KI / ethanol / Heating

With lithium aluminium tetrahydride; potassium carbonate; potassium iodide; In ethanol;