3-{[(benzyloxy)carbonyl]amino}-7-(4-methylpiperazin-1-yl)quinoline-2-carboxylic acid

Base Information

Chemical Name:3-{[(benzyloxy)carbonyl]amino}-7-(4-methylpiperazin-1-yl)quinoline-2-carboxylic acid
CAS No.:1620240-25-6
Molecular Formula:C₂₃H₂₄N₄O₄
Molecular Weight:420.468
Hs Code.:

Synonyms:3-{[(benzyloxy)carbonyl]amino}-7-(4-methylpiperazin-1-yl)quinoline-2-carboxylic acid

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Chemical Property of 3-{[(benzyloxy)carbonyl]amino}-7-(4-methylpiperazin-1-yl)quinoline-2-carboxylic acid

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Technology Process of 3-{[(benzyloxy)carbonyl]amino}-7-(4-methylpiperazin-1-yl)quinoline-2-carboxylic acid

There total 4 articles about 3-{[(benzyloxy)carbonyl]amino}-7-(4-methylpiperazin-1-yl)quinoline-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₈N₄O₄

: 1620240-25-6
3-{[(benzyloxy)carbonyl]amino}-7-(4-methylpiperazin-1-yl)quinoline-2-carboxylic acid

Guidance literature:: C₂₅H₂₈N₄O₄; With sodium hydroxide; In 1,4-dioxane; at 80 ℃; for 0.5h;

With water;

Reference yield:

: 1260807-99-5
ethyl 3-amino-7-bromoquinoline-2-carboxylate

: 1620240-25-6
3-{[(benzyloxy)carbonyl]amino}-7-(4-methylpiperazin-1-yl)quinoline-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / -10 - 20 °C

2: potassium phosphate; palladium diacetate; ruphos / tert-butyl alcohol / 2 h / 100 °C / Inert atmosphere; Sealed tube

3: sodium hydroxide / 1,4-dioxane / 0.5 h / 80 °C

With pyridine; potassium phosphate; palladium diacetate; sodium hydroxide; ruphos; In 1,4-dioxane; dichloromethane; tert-butyl alcohol;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1620240-25-6
3-{[(benzyloxy)carbonyl]amino}-7-(4-methylpiperazin-1-yl)quinoline-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / -10 - 20 °C

2: potassium phosphate; palladium diacetate; ruphos / tert-butyl alcohol / 2 h / 100 °C / Inert atmosphere; Sealed tube

3: sodium hydroxide / 1,4-dioxane / 0.5 h / 80 °C

With pyridine; potassium phosphate; palladium diacetate; sodium hydroxide; ruphos; In 1,4-dioxane; dichloromethane; tert-butyl alcohol;