ethyl N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate

Base Information

Chemical Name:ethyl N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate
CAS No.:865805-03-4
Molecular Formula:C₂₇H₃₀Br₂N₂O₂
Molecular Weight:574.355
Hs Code.:

Synonyms:ethyl N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate

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Technology Process of ethyl N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate

There total 1 articles about ethyl N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 181219-01-2
4-pyridineboronic acid pinacol ester

: 763110-65-2
ethyl N-[(2,4,6-tribromophenyl)(4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate

: 865805-03-4
ethyl N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate

Guidance literature:: With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; at 100 ℃; for 48h;
DOI:10.1021/jo0504363

Reference yield: 86.0%

: 865805-03-4
ethyl N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate

: 865805-04-5
ethyl N-nitroso-N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate

Guidance literature:: With acetic anhydride; acetic acid; sodium nitrite; at 0 - 20 ℃;
DOI:10.1021/jo0504363

Reference yield:

: 865805-03-4
ethyl N-[[2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)methyl]carbamate

: [2,6-dibromo-4-(4-pyridyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)ketone

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / sodium nitrite; acetic anhydride; acetic acid / 0 - 20 °C

2: 21 percent / t-BuOK / tetrahydrofuran / -20 °C

3: O₂ / benzene / Irradiation

With potassium tert-butylate; oxygen; acetic anhydride; acetic acid; sodium nitrite; In tetrahydrofuran; benzene;
DOI:10.1021/jo0504363