[1-(5,8-dimethyl-[1,2,4]triazolo[1,5-a]pyrazin-2-yl)ethyl]triphenyl phosphonium chloride

Base Information

Chemical Name:[1-(5,8-dimethyl-[1,2,4]triazolo[1,5-a]pyrazin-2-yl)ethyl]triphenyl phosphonium chloride
CAS No.:1447715-68-5
Molecular Formula:C₂₇H₂₆N₄P*Cl
Molecular Weight:472.957
Hs Code.:

Synonyms:[1-(5,8-dimethyl-[1,2,4]triazolo[1,5-a]pyrazin-2-yl)ethyl]triphenyl phosphonium chloride

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Chemical Property of [1-(5,8-dimethyl-[1,2,4]triazolo[1,5-a]pyrazin-2-yl)ethyl]triphenyl phosphonium chloride

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Technology Process of [1-(5,8-dimethyl-[1,2,4]triazolo[1,5-a]pyrazin-2-yl)ethyl]triphenyl phosphonium chloride

There total 2 articles about [1-(5,8-dimethyl-[1,2,4]triazolo[1,5-a]pyrazin-2-yl)ethyl]triphenyl phosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.7%

: 1447715-66-3
2-(1-chloroethyl)-5,8-dimethyl-[1,2,4]triazolo[1,5-a]pyrazine

: 603-35-0
triphenylphosphine

: 1447715-68-5
[1-(5,8-dimethyl-[1,2,4]triazolo[1,5-a]pyrazin-2-yl)ethyl]triphenyl phosphonium chloride

Guidance literature:: In acetonitrile; at 200 ℃; for 4h; Microwave irradiation;

Reference yield:

: 13134-38-8
3,6-dimethylpyrazin-2-yl amine

: 1447715-68-5
[1-(5,8-dimethyl-[1,2,4]triazolo[1,5-a]pyrazin-2-yl)ethyl]triphenyl phosphonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: mesitylenesulfonylhydroxylamine / dichloromethane / 0.25 h / 20 °C / Cooling with ice

1.2: 0.08 h / 20 °C

1.3: 48 h / 20 °C

2.1: acetonitrile / 4 h / 200 °C / Microwave irradiation

With mesitylenesulfonylhydroxylamine; In dichloromethane; acetonitrile;