6-bromo-3-isopropoxy-2-methoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide

Base Information

Chemical Name:6-bromo-3-isopropoxy-2-methoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide
CAS No.:511545-64-5
Molecular Formula:C₂₂H₂₀BrNO₅
Molecular Weight:458.308
Hs Code.:

Synonyms:6-bromo-3-isopropoxy-2-methoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide

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Chemical Property of 6-bromo-3-isopropoxy-2-methoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide

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Technology Process of 6-bromo-3-isopropoxy-2-methoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide

There total 3 articles about 6-bromo-3-isopropoxy-2-methoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 53811-49-7
naphtho[2,3-d][1,3]dioxol-5-amine

: 511545-66-7
6-bromo-3-isopropoxy-2-methoxybenzoic acid

: 511545-64-5
6-bromo-3-isopropoxy-2-methoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide

Guidance literature:: 6-bromo-3-isopropoxy-2-methoxybenzoic acid; With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; for 1h; Heating;

naphtho[2,3-d][1,3]dioxol-5-amine; With triethylamine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.3987/COM-02-S35

Reference yield:

: 218903-24-3
3-isopropoxy-2-methoxybenzaldehyde

: 511545-64-5
6-bromo-3-isopropoxy-2-methoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 89 percent / sodium phosphate dihydrate; hydrogen peroxide; sodium chlorite / acetonitrile; H₂O / 8 h / 10 °C

2.1: 80 percent / NaOH; dibromodimethylhydantoin / H₂O / 0.67 h / 20 °C

3.1: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 1 h / Heating

3.2: 78 percent / NEt₃ / CH₂Cl₂ / 5 h / 20 °C

With sodium hydroxide; sodium chlorite; disodium hydrogenphosphate; oxalyl dichloride; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; dihydrogen peroxide; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3987/COM-02-S35

Reference yield:

: 85747-57-5
3-isopropoxy-2-methoxybenzoic acid

: 511545-64-5
6-bromo-3-isopropoxy-2-methoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 80 percent / NaOH; dibromodimethylhydantoin / H₂O / 0.67 h / 20 °C

2.1: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 1 h / Heating

2.2: 78 percent / NEt₃ / CH₂Cl₂ / 5 h / 20 °C

With sodium hydroxide; oxalyl dichloride; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.3987/COM-02-S35