Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid

Base Information

Chemical Name:Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid
CAS No.:106948-02-1
Molecular Formula:C₂₃H₂₄N₂O₈S
Molecular Weight:488.518
Hs Code.:

Synonyms:Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid

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Chemical Property of Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid

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Technology Process of Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid

There total 6 articles about Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 106947-93-7
Methyl-5,6-anhydro-2-benzamido-2-desoxy-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid

: 106948-02-1
Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid

Guidance literature:: With triphenylphosphine sulfide; trifluoroacetic acid; In chloroform; at 50 ℃; for 12h;

Reference yield:

: 106947-89-1
Methyl-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-β-D-glucofuranosid

: 106948-02-1
Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / pyridine / 12 h / 0 °C

2: 86 percent / aq. NaOH / tetrahydrofuran / 2 h / 0 °C

3: 50 percent / DCC / ethyl acetate / 1.) 0 deg C, 30 min, 2.) room temp., 6 h

4: 42 percent / (C₆H₅)3PS, CF₃COOH / CHCl₃ / 12 h / 50 °C

With pyridine; sodium hydroxide; dicyclohexyl-carbodiimide; triphenylphosphine sulfide; trifluoroacetic acid; In tetrahydrofuran; chloroform; ethyl acetate;

Reference yield:

: 3804-93-1
(R)-2-[(3aR,5S,6R,6aR)-5-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazol-6-yloxy]-propionic acid

: 106948-02-1
Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / 168 h / Ambient temperature

2: 86 percent / 60percent aq. CH₃COOH / 23 h / Ambient temperature

3: 73 percent / pyridine / 12 h / 0 °C

4: 86 percent / aq. NaOH / tetrahydrofuran / 2 h / 0 °C

5: 50 percent / DCC / ethyl acetate / 1.) 0 deg C, 30 min, 2.) room temp., 6 h

6: 42 percent / (C₆H₅)3PS, CF₃COOH / CHCl₃ / 12 h / 50 °C

With pyridine; sodium hydroxide; acetic acid; dicyclohexyl-carbodiimide; triphenylphosphine sulfide; trifluoroacetic acid; In tetrahydrofuran; chloroform; ethyl acetate;