2-{[(3,3-diethoxypropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester

Base Information

Chemical Name:2-{[(3,3-diethoxypropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester
CAS No.:940279-24-3
Molecular Formula:C₂₀H₃₁NO₆S
Molecular Weight:413.535
Hs Code.:

Synonyms:2-{[(3,3-diethoxypropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester

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Chemical Property of 2-{[(3,3-diethoxypropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester

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Technology Process of 2-{[(3,3-diethoxypropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester

There total 1 articles about 2-{[(3,3-diethoxypropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 164532-58-5
N-(p-tosyl)-3-aminopropionaldehyde diethyl acetal

: 17435-72-2
ethyl 2-bromomethyl-2-propenoate

: 940279-24-3
2-{[(3,3-diethoxypropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1021/ol070482k

Reference yield: 74.0%

: 940279-24-3
2-{[(3,3-diethoxypropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester

: 940279-28-7
2-{[(3-oxopropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester

Guidance literature:: With hydrogenchloride; acetic acid; at 0 - 5 ℃; for 1h;
DOI:10.1021/ol070482k

Reference yield:

: 940279-24-3
2-{[(3,3-diethoxypropyl)-(toluene-4-sulfonyl)-amino]-methyl}-acrylic acid ethyl ester

: (+/-)-(3R,4S)-4-hydroxy-3-iodomethyl-1-(toluene-4-sulfonyl)-pyperidine-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / aq. HCl; AcOH / 1 h / 0 - 5 °C

2: 74 percent / TiCl₄; Bu₄NI / CH₂Cl₂ / 1 h / 0 °C

With hydrogenchloride; titanium tetrachloride; tetra-(n-butyl)ammonium iodide; acetic acid; In dichloromethane;
DOI:10.1021/ol070482k