C₃₇H₅₉BrN₂O₈S

Base Information

Chemical Name:C₃₇H₅₉BrN₂O₈S
CAS No.:1437119-02-2
Molecular Formula:C₃₇H₅₉BrN₂O₈S
Molecular Weight:771.854
Hs Code.:

C<sub>37</sub>H<sub>59</sub>BrN<sub>2</sub>O<sub>8</sub>S

Synonyms:C₃₇H₅₉BrN₂O₈S

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Chemical Property of C₃₇H₅₉BrN₂O₈S

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Technology Process of C₃₇H₅₉BrN₂O₈S

There total 22 articles about C₃₇H₅₉BrN₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1437118-97-2
C₃₀H₅₁BrO₇

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1437119-02-2
C₃₇H₅₉BrN₂O₈S

Guidance literature:: In methanol; at 45 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.041

Reference yield:

: C₂₁H₃₄O₅

: 1437119-02-2
C₃₇H₅₉BrN₂O₈S

Guidance literature:: Multi-step reaction with 10 steps

1.1: lithium hydroxide / tetrahydrofuran; methanol / 0.5 h / 0 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / -78 °C / Inert atmosphere

3.1: triethylamine; dmap / dichloromethane / 20 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; ozone; oxygen / dichloromethane; methanol / -78 °C / Inert atmosphere

5.1: Schwartz's reagent / dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Darkness

5.2: 0.25 h / -78 °C / Inert atmosphere; Darkness

5.3: -78 - 20 °C / Inert atmosphere; Darkness

6.1: palladium 10% on activated carbon; hydrogen / ethanol / 1.5 h / 20 °C / Inert atmosphere

7.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

8.1: tetrahydrofuran; diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

9.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

10.1: methanol / 18 h / 45 °C / Inert atmosphere

With dmap; Schwartz's reagent; tetrapropylammonium perruthennate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; oxygen; sodium hydrogencarbonate; ozone; 4-methylmorpholine N-oxide; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane;
DOI:10.1016/j.tet.2013.04.041

Reference yield:

: C₃₄H₆₁BrO₈Si

: 1437119-02-2
C₃₇H₅₉BrN₂O₈S

Guidance literature:: Multi-step reaction with 4 steps

1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

2: tetrahydrofuran; diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

3: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

4: methanol / 18 h / 45 °C / Inert atmosphere

With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2013.04.041