1,3-diethyl 2-({[3,4-bis(2-methoxyethoxy)phenyl]amino}methylidene)propanedioate

Base Information

Chemical Name:1,3-diethyl 2-({[3,4-bis(2-methoxyethoxy)phenyl]amino}methylidene)propanedioate
CAS No.:1219717-67-5
Molecular Formula:C₂₀H₂₉NO₈
Molecular Weight:411.452
Hs Code.:

Synonyms:1,3-diethyl 2-({[3,4-bis(2-methoxyethoxy)phenyl]amino}methylidene)propanedioate

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Chemical Property of 1,3-diethyl 2-({[3,4-bis(2-methoxyethoxy)phenyl]amino}methylidene)propanedioate

Chemical Property:

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Technology Process of 1,3-diethyl 2-({[3,4-bis(2-methoxyethoxy)phenyl]amino}methylidene)propanedioate

There total 3 articles about 1,3-diethyl 2-({[3,4-bis(2-methoxyethoxy)phenyl]amino}methylidene)propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,4-bis(2-methoxyethoxy) aniline

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 1219717-67-5
1,3-diethyl 2-({[3,4-bis(2-methoxyethoxy)phenyl]amino}methylidene)propanedioate

Guidance literature:: at 100 ℃; for 3h;
DOI:10.1021/jm901877j

Reference yield:

: 3316-09-4
1,2-dihydroxy-4-nitrobenzene

: 1219717-67-5
1,3-diethyl 2-({[3,4-bis(2-methoxyethoxy)phenyl]amino}methylidene)propanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C

2: palladium on activated charcoal; hydrogen / methanol / 8 h / 20 °C

3: 3 h / 100 °C

With palladium on activated charcoal; hydrogen; potassium carbonate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 33311-30-7
1,2-bis (2-methoxyethoxy)-4-nitrobenzene

: 1219717-67-5
1,3-diethyl 2-({[3,4-bis(2-methoxyethoxy)phenyl]amino}methylidene)propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / methanol / 8 h / 20 °C

2: 3 h / 100 °C

With palladium on activated charcoal; hydrogen; In methanol;