Technology Process of C36H50N2O7SSi
There total 8 articles about C36H50N2O7SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine;
In
1,4-dioxane;
at 100 ℃;
for 21h;
DOI:10.1002/ejoc.201100242
- Guidance literature:
-
Multi-step reaction with 6 steps
1: acetic acid; zinc / water / 1.83 h / 80 - 85 °C
2: glyoxylic acid ethyl ester; magnesium sulfate / dichloromethane / 0 - 20 °C
3: dmap; triethylamine / toluene / 18 h / 70 °C
4: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C
5: dichloromethane / 4 h / 20 °C
6: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 1,4-dioxane / 21 h / 100 °C
With
dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); glyoxylic acid ethyl ester; ammonium cerium (IV) nitrate; magnesium sulfate; acetic acid; triethylamine; zinc;
In
1,4-dioxane; dichloromethane; water; toluene; acetonitrile;
6: Sonogashira coupling;
DOI:10.1002/ejoc.201100242
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; triethylamine / toluene / 18 h / 70 °C
2: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C
3: dichloromethane / 4 h / 20 °C
4: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 1,4-dioxane / 21 h / 100 °C
With
dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); ammonium cerium (IV) nitrate; triethylamine;
In
1,4-dioxane; dichloromethane; water; toluene; acetonitrile;
4: Sonogashira coupling;
DOI:10.1002/ejoc.201100242
