(2R,3R,4R,5S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-7-vinyl-1,2,3,4,5-heptanepentol

Base Information

Chemical Name:(2R,3R,4R,5S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-7-vinyl-1,2,3,4,5-heptanepentol
CAS No.:595559-99-2
Molecular Formula:C₄₄H₄₉NO₅
Molecular Weight:671.877
Hs Code.:

Synonyms:(2R,3R,4R,5S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-7-vinyl-1,2,3,4,5-heptanepentol

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Chemical Property of (2R,3R,4R,5S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-7-vinyl-1,2,3,4,5-heptanepentol

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Technology Process of (2R,3R,4R,5S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-7-vinyl-1,2,3,4,5-heptanepentol

There total 7 articles about (2R,3R,4R,5S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-7-vinyl-1,2,3,4,5-heptanepentol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 166111-63-3
N-benzyl-2,3,4,6-tetra-O-benzyl-D-glucopyranosylamine

: 1730-25-2
allylmagnesium bromide

: 595559-99-2
(2R,3R,4R,5S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-7-vinyl-1,2,3,4,5-heptanepentol

Guidance literature:: In diethyl ether;
DOI:10.1039/b003877f

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 595559-99-2
(2R,3R,4R,5S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-7-vinyl-1,2,3,4,5-heptanepentol

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / 0.75 h / 110 °C

2: 85 percent / diethyl ether; tetrahydrofuran / 3.5 h / -30 °C

3: Cu(OCOCH₃)2*H₂O; acetic acid; Zn / H₂O / 1 h / 20 - 70 °C

With copper diacetate; acetic acid; zinc; In tetrahydrofuran; diethyl ether; water;
DOI:10.1016/S0040-4020(03)00631-8